Benzenemethanol, 4-hexyl-a-methyl-

Base Information

• Chemical Name: Benzenemethanol, 4-hexyl-a-methyl-
• CAS No.: 100963-63-1
• Molecular Formula: C14H22O
• Molecular Weight: 206.32400
• Mol file: 100963-63-1.mol

Synonyms:1-(4-Hexyl-phenyl)-ethanol;1-(4-Hexyl-phenyl)-aethanol;

Chemical Property of Benzenemethanol, 4-hexyl-a-methyl-

Chemical Property:

• Boiling Point: 119 - 120 °C (2 mmHg)
• PSA: 20.23000
• LogP: 3.86270

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Benzenemethanol, 4-hexyl-a-methyl-

There total 2 articles about Benzenemethanol, 4-hexyl-a-methyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-(4-hexyl-phenyl)-ethanone (37592-72-6) → 1-(4-hexyl-phenyl)-ethanol (100963-63-1)

Guidance literature:

With aluminum isopropoxide; isopropyl alcohol;

DOI:10.1021/ja01110a010

Reference yield:

hexylbenzene (1077-16-3) → 1-(4-hexyl-phenyl)-ethanol (100963-63-1)

Guidance literature:

Multi-step reaction with 2 steps

1: AlCl₃ / CH₂Cl₂ / 5 h / 20 °C

2: NaBH₄ / methanol / 2 h / 20 °C

With sodium tetrahydroborate; aluminium trichloride; In methanol; dichloromethane;

DOI:10.1021/ma035947a

Reference yield: 65.0%

1-(4-hexyl-phenyl)-ethanol (100963-63-1) → 1-hexyl-4-vinylbenzene (10074-43-8)

Guidance literature:

With toluene-4-sulfonic acid; In toluene; for 2h; Heating;

DOI:10.1021/ma035947a

upstream raw materials:

1-(4-hexyl-phenyl)-ethanone

hexylbenzene

Downstream raw materials:

1-hexyl-4-vinylbenzene

Refernces

• 1、 Quirk, Roderic P.,Ok, Myung-Ahn. "Syndiospecific synthesis of longer p-n-alkyl-substituted polystyrenes using monocyclopentadienyl-type titanium catalysts". . p. 3976 - 3982. Retrieved 2007/10/03.