Technology Process of 1,2-Benzenediol, 4,4'-(1,3-propanediyl)bis-
There total 6 articles about 1,2-Benzenediol, 4,4'-(1,3-propanediyl)bis- which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: palladium/CaCO3; ethyl acetate; ethanol / Hydrogenation
2: amalgamated zinc; aqueous HCl; acetic acid / Reagens 4: Toluol
3: aqueous HI; acetic acid
With
hydrogenchloride; Lindlar's catalyst; amalgamated zinc; ethanol; hydrogen iodide; acetic acid; ethyl acetate;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: sodium hydroxide / ethanol / 6 h / 75 °C
2: palladium on activated charcoal; hydrogen / methanol; ethyl acetate / 24 h / 20 °C
3: sodium tetrahydroborate / methanol / 1 h / 0 °C
4: sulfuric acid / 5 h / Reflux
5: palladium on activated charcoal; hydrogen / methanol; ethyl acetate / 24 h / 20 °C
6: boron tribromide / dichloromethane / 1 h / -78 - 20 °C
With
sodium tetrahydroborate; sulfuric acid; palladium on activated charcoal; hydrogen; boron tribromide; sodium hydroxide;
In
methanol; ethanol; dichloromethane; ethyl acetate;
DOI:10.1016/j.ejmech.2019.111910