N,N'-[Ethene-1,2-diyldi(4,1-phenylene)]bis[N-(4-methoxyphenyl)aniline]

Base Information

Chemical Name:N,N'-[Ethene-1,2-diyldi(4,1-phenylene)]bis[N-(4-methoxyphenyl)aniline]
CAS No.:101186-93-0
Molecular Formula:C40H34N2O2
Molecular Weight:574.71000
Hs Code.:
DSSTox Substance ID:DTXSID40709762
Mol file:101186-93-0.mol

Synonyms:101186-93-0;DTXSID40709762;N,N'-[Ethene-1,2-diyldi(4,1-phenylene)]bis[N-(4-methoxyphenyl)aniline]

Suppliers and Price of N,N'-[Ethene-1,2-diyldi(4,1-phenylene)]bis[N-(4-methoxyphenyl)aniline]

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N,N'-[Ethene-1,2-diyldi(4,1-phenylene)]bis[N-(4-methoxyphenyl)aniline]

Chemical Property:

Boiling Point:734.3±60.0 °C(Predicted)
PSA：24.94000
Density:1.189±0.06 g/cm3(Predicted)
LogP:10.81380
XLogP3:10.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:10
Exact Mass:574.262028332
Heavy Atom Count:44
Complexity:750

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:COC1=CC=C(C=C1)N(C2=CC=CC=C2)C3=CC=C(C=C3)C=CC4=CC=C(C=C4)N(C5=CC=CC=C5)C6=CC=C(C=C6)OC

Technology Process of N,N'-[Ethene-1,2-diyldi(4,1-phenylene)]bis[N-(4-methoxyphenyl)aniline]

There total 3 articles about N,N'-[Ethene-1,2-diyldi(4,1-phenylene)]bis[N-(4-methoxyphenyl)aniline] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 87755-82-6
4-[N-phenyl-N-(4-methoxyphenyl)amino]benzaldehyde

: 101186-93-0
p,p'-bis[N-(4-methoxyphenyl)-N-phenylamino]stilbene

Guidance literature:: With pyridine; titanium tetrachloride; zinc; In tetrahydrofuran; at -15 ℃; for 2h; Reflux;
DOI:10.1002/ejoc.201100821

Reference yield: 22.0%

: 1351663-33-6
diethyl 4-[N-(4-methoxyphenyl)-N-phenylamino]benzylphosphonate

: 87755-82-6
4-[N-phenyl-N-(4-methoxyphenyl)amino]benzaldehyde

: 101186-93-0
p,p'-bis[N-(4-methoxyphenyl)-N-phenylamino]stilbene

Guidance literature:: diethyl 4-[N-(4-methoxyphenyl)-N-phenylamino]benzylphosphonate; With potassium tert-butylate; In tetrahydrofuran; for 0.5h; Cooling with ice;

4-[N-phenyl-N-(4-methoxyphenyl)amino]benzaldehyde; In tetrahydrofuran; at 0 - 20 ℃; for 24h;
DOI:10.1002/ejoc.201100821

Reference yield:

: 521950-74-3
4-[N-(4-methoxyphenyl)-N-phenylamino]benzyl alcohol

: 101186-93-0
p,p'-bis[N-(4-methoxyphenyl)-N-phenylamino]stilbene

Guidance literature:: Multi-step reaction with 2 steps

1.1: iodine / 0 - 20 °C

2.1: potassium tert-butylate / tetrahydrofuran / 0.5 h / Cooling with ice

2.2: 24 h / 0 - 20 °C

With potassium tert-butylate; iodine; In tetrahydrofuran; 2.1: Horner-Wittig condensation / 2.2: Horner-Wittig condensation;
DOI:10.1002/ejoc.201100821