N-Phenyl-2H-1,3,2-benzodioxaphosphol-2-amine

Base Information

Chemical Name:N-Phenyl-2H-1,3,2-benzodioxaphosphol-2-amine
CAS No.:10154-54-8
Molecular Formula:C12H10NO2P
Molecular Weight:231.191
Hs Code.:
DSSTox Substance ID:DTXSID10502222
Wikidata:Q82355075
Mol file:10154-54-8.mol

Synonyms:DTXSID10502222;10154-54-8;N-Phenyl-2H-1,3,2-benzodioxaphosphol-2-amine

Suppliers and Price of N-Phenyl-2H-1,3,2-benzodioxaphosphol-2-amine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 0 raw suppliers

Chemical Property of N-Phenyl-2H-1,3,2-benzodioxaphosphol-2-amine

Chemical Property:

XLogP3:3.6
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:2
Exact Mass:231.04491556
Heavy Atom Count:16
Complexity:219

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)NP2OC3=CC=CC=C3O2

Technology Process of N-Phenyl-2H-1,3,2-benzodioxaphosphol-2-amine

There total 1 articles about N-Phenyl-2H-1,3,2-benzodioxaphosphol-2-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1641-40-3
pyrocatechol phosphorochloridite

: 62-53-3
aniline

: 10154-54-8
Brenzcatechylphosphorigsaureester-anilid

Guidance literature:: With triethylamine; In benzene;

Reference yield: 25.0%

: 10154-54-8
Brenzcatechylphosphorigsaureester-anilid

: 4918-98-3
phosphoric acid 2-hydroxyphenyl phosphate

: 4846-23-5
pyrocatechol cyclophosphoric acid

Guidance literature:: With chlorhexidine diphosphanilate; In chlorobenzene; at 30 ℃; Product distribution; Mechanism; subst. effects;

Reference yield:

: 10154-54-8
Brenzcatechylphosphorigsaureester-anilid

: C₆H₄O₂PSSe^(1-)*Na⁽¹⁺⁾

: 103-72-0
phenyl isothiocyanate

Guidance literature:: Multi-step reaction with 2 steps

1: selenium / toluene / Inert atmosphere; Heating; Sealed ampoule

2: sodium hydride / ⁽²⁾H₈-toluene; N,N-dimethyl-formamide / -40 °C / Inert atmosphere; Cooling with liquid nitrogen

With selenium; sodium hydride; In ⁽²⁾H₈-toluene; N,N-dimethyl-formamide; toluene; 2: Stec reaction;
DOI:10.1016/j.tet.2012.04.081