1H-Isoindole-1,3(2H)-dione, 2-(2,3-dihydro-1,5-dimethyl-3-oxo-2-phenyl-1H-pyrazol-4-yl)-

Base Information

Chemical Name:1H-Isoindole-1,3(2H)-dione, 2-(2,3-dihydro-1,5-dimethyl-3-oxo-2-phenyl-1H-pyrazol-4-yl)-
CAS No.:101896-02-0
Molecular Formula:C19H15N3O3
Molecular Weight:333.346
Hs Code.:
Mol file:101896-02-0.mol

Synonyms:N-(1,5-Dimethyl-3-oxo-2-phenyl-2,3-dihydro-1H-pyrazol-4-yl)-phthalimid;N-antipyrine-phthalimide;2-(1,5-Dimethyl-3-oxo-2-phenyl-2,3-dihydro-1H-pyrazol-4-yl)-isoindole-1,3-dione;N-(1,5-dimethyl-3-oxo-2-phenyl-2,3-dihydro-1H-pyrazol-4-yl)-phthalimide;

Suppliers and Price of 1H-Isoindole-1,3(2H)-dione, 2-(2,3-dihydro-1,5-dimethyl-3-oxo-2-phenyl-1H-pyrazol-4-yl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 1H-Isoindole-1,3(2H)-dione, 2-(2,3-dihydro-1,5-dimethyl-3-oxo-2-phenyl-1H-pyrazol-4-yl)-

Chemical Property:

Melting Point:206-208 °C
Boiling Point:485.9±55.0 °C(Predicted)
PSA：64.31000
Density:1.406±0.06 g/cm3(Predicted)
LogP:2.35000

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1H-Isoindole-1,3(2H)-dione, 2-(2,3-dihydro-1,5-dimethyl-3-oxo-2-phenyl-1H-pyrazol-4-yl)-

There total 4 articles about 1H-Isoindole-1,3(2H)-dione, 2-(2,3-dihydro-1,5-dimethyl-3-oxo-2-phenyl-1H-pyrazol-4-yl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.56%

: 19357-14-3
N-antipyrine-phthalamic acid

: 101896-02-0
4-(1,3-dioxoisoindolin-2-yl)antipyrine

Guidance literature:: In acetic acid; Heating;

Reference yield: 61.0%

: 85-44-9
phthalic anhydride

: 83-07-8
4-amino-2,3-dimethyl-1-phenylpyrazolin-5-one

: 101896-02-0
4-(1,3-dioxoisoindolin-2-yl)antipyrine

Guidance literature:: phthalic anhydride; 4-amino-2,3-dimethyl-1-phenylpyrazolin-5-one; In ethanol; at 0 ℃; for 0.25h;

With triethylamine; In ethanol; Reflux;
DOI:10.1016/j.molstruc.2012.03.021

Reference yield:

: 85-44-9
phthalic anhydride

: 101896-02-0
4-(1,3-dioxoisoindolin-2-yl)antipyrine

Guidance literature:: Multi-step reaction with 2 steps

1: 79.75 percent / diethyl ether

2: 87.56 percent / acetic acid / Heating

In diethyl ether; acetic acid;