β-Phenylhydrocinnamic acid hydrazide

Base Information

• Chemical Name: β-Phenylhydrocinnamic acid hydrazide
• CAS No.: 58973-41-4
• Molecular Formula: C15H16N2O
• Molecular Weight: 240.305
• Hs Code.: 2928000090
• Mol file: 58973-41-4.mol

Synonyms:3,3-diphenylpropionic acid hydrazide;3,3-Diphenyl-propionsaeure-hydrazid;3,3-diphenylpropanohydrazide;

Chemical Property of β-Phenylhydrocinnamic acid hydrazide

Chemical Property:

• Vapor Pressure: 9.75E-09mmHg at 25°C
• Boiling Point: 462.6°C at 760 mmHg
• Flash Point: 233.6°C
• PSA: 55.12000
• Density: 1.132g/cm³
• LogP: 3.28970

Purity/Quality:

98%min ^*data from raw suppliers

3,3-Diphenylpropanohydrazide ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of β-Phenylhydrocinnamic acid hydrazide

There total 2 articles about β-Phenylhydrocinnamic acid hydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3,3-diphenyl-propionic acid ethyl ester (7476-18-8) → 3,3-diphenylpropionic acid hydrazide (58973-41-4)

Guidance literature:

With hydrazine hydrate; In methanol; for 3h; Heating;

DOI:10.1248/cpb.31.2810

Reference yield:

→ 3,3-diphenylpropionic acid hydrazide (58973-41-4)

Guidance literature:

With ethanol; hydrazine hydrate;

Reference yield:

ethyl 3-{[(lE,Z)-chloro(3-fluorophenyl)methylene]amino}benzoate + 3,3-diphenylpropionic acid hydrazide (58973-41-4) → ethyl 3-[3-(2,2-diphenylethyl)-5-(3-fluorophenyl)-4H-1,2,4-triazol-4-yl]benzoate

Guidance literature:

In acetonitrile; at 90 ℃; for 16h;

upstream raw materials:

3,3-diphenyl-propionic acid ethyl ester

Downstream raw materials:

(2,2-diphenyl-ethyl)-carbamic acid ethyl ester

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