2-Amino-4-hydroxy-3,5-diiodobenzonitrile

Base Information

Chemical Name:2-Amino-4-hydroxy-3,5-diiodobenzonitrile
CAS No.:102569-30-2
Molecular Formula:C7H4I2N2O
Molecular Weight:385.931
Hs Code.:
DSSTox Substance ID:DTXSID20541501
Wikidata:Q82417873
Mol file:102569-30-2.mol

Synonyms:2-Amino-4-hydroxy-3,5-diiodobenzonitrile;102569-30-2;DTXSID20541501

Suppliers and Price of 2-Amino-4-hydroxy-3,5-diiodobenzonitrile

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2-Amino-4-hydroxy-3,5-diiodobenzonitrile

Chemical Property:

XLogP3:2.5
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:0
Exact Mass:385.84131
Heavy Atom Count:12
Complexity:215

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=C(C(=C(C(=C1I)O)I)N)C#N

Technology Process of 2-Amino-4-hydroxy-3,5-diiodobenzonitrile

There total 2 articles about 2-Amino-4-hydroxy-3,5-diiodobenzonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 67608-59-7
2-Amino-4-hydroxy-benzonitril

: 102569-30-2
2-Amino-3,5-diiodo-4-hydroxy-benzonitril

Guidance literature:: With iodine; iodic acid; In ethanol; for 1h; Heating;
DOI:10.1055/s-1985-31345

Reference yield:

: 72817-93-7
4-Amino-5-cyano-salicylsaeure

: 102569-30-2
2-Amino-3,5-diiodo-4-hydroxy-benzonitril

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / quinoline / 0.75 h / 170 - 180 °C

2: 75 percent / I₂/HIO₃ / aq. ethanol / 1 h / Heating

With iodine; iodic acid; In quinoline; ethanol;
DOI:10.1055/s-1985-31345

Reference yield:

: 102569-30-2
2-Amino-3,5-diiodo-4-hydroxy-benzonitril

: 111698-42-1
3,5-diiodo-2-chloro-4-hydroxybenzonitrile

Guidance literature:: With hydrogenchloride; sulfuric acid; copper(l) chloride; sodium nitrite; Yield given. Multistep reaction; 1) glacial acetic acid, RT, 2) 60 - 70 deg C;
DOI:10.1007/BF00810055