3-methyl-2,2'-bipyridine

Base Information

• Chemical Name: 3-methyl-2,2'-bipyridine
• CAS No.: 10273-88-8
• Molecular Formula: C11H10N2
• Molecular Weight: 170.214
• Mol file: 10273-88-8.mol

Synonyms:3-methyl-2,2’-bipyridine;3-methyl-[2,2']bipyridinyl;6'-methyl-2,2'-dipyridyl;3-methyl-2,2'-bipyridyl;3-Methyl-dipyridyl-(2,2');6-methyl-2,2'-bipyridine;

Chemical Property of 3-methyl-2,2'-bipyridine

Chemical Property:

• Boiling Point: 148 - 156 °C (5 mmHg)
• PKA: 4.39±0.20(Predicted)
• PSA: 25.78000
• Density: 1.081±0.06 g/cm3(Predicted)
• LogP: 2.45200

Purity/Quality:

98%,99%, ^*data from raw suppliers

3-Methyl-[2,2']bipyridinyl 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-methyl-2,2'-bipyridine

There total 9 articles about 3-methyl-2,2'-bipyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

2-bromo-3-picoline (3430-17-9) + pyridine-2-boronic acid N-phenyldiethanolamine ester (882521-96-2) → 3-methyl-2,2'-bipyridine (10273-88-8)

Guidance literature:

With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In tetrahydrofuran; for 24h; Reflux; Inert atmosphere;

DOI:10.1055/s-0029-1217082

Reference yield: 89.0%

2-Cyano-6-methylpyridine (1620-75-3) + Glyoxal (131543-46-9,107-22-2) + bicyclo[2.2.1]hepta-2,5-diene (121-46-0) → 3-methyl-2,2'-bipyridine (10273-88-8)

Guidance literature:

With hydrazine hydrate; In water;

Reference yield: 89.0%

C9H8N4 → 3-methyl-2,2'-bipyridine (10273-88-8)

Guidance literature:

With bicyclo[2.2.1]hepta-2,5-diene; for 3h; Heating / reflux;

upstream raw materials:

2-bromo-3-picoline

2-Cyano-6-methylpyridine

Glyoxal

bicyclo[2.2.1]hepta-2,5-diene

Downstream raw materials:

C₂₉H₃₁BN₂

C₂₀H₁₉BN₂

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 10273-88-8 3-methyl-2,2'-bipyridine

Send

Send

Metric Ton KG G Pound L ML

Send

Send