6H-Purin-6-one, 1,9-dihydro-9-[(2-hydroxyethoxy)methyl]-2-[[(4-methoxyphenyl)diphenyl methyl]amino]-

Base Information

Chemical Name:6H-Purin-6-one, 1,9-dihydro-9-[(2-hydroxyethoxy)methyl]-2-[[(4-methoxyphenyl)diphenyl methyl]amino]-
CAS No.:103024-95-9
Molecular Formula:C28H27N5O4
Molecular Weight:497.553
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 6H-Purin-6-one, 1,9-dihydro-9-[(2-hydroxyethoxy)methyl]-2-[[(4-methoxyphenyl)diphenyl methyl]amino]-

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:: SDS file from LookChem

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Technology Process of 6H-Purin-6-one, 1,9-dihydro-9-[(2-hydroxyethoxy)methyl]-2-[[(4-methoxyphenyl)diphenyl methyl]amino]-

There total 3 articles about 6H-Purin-6-one, 1,9-dihydro-9-[(2-hydroxyethoxy)methyl]-2-[[(4-methoxyphenyl)diphenyl methyl]amino]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 59277-89-3
acycloguanosine

: 14470-28-1
mono-4-methoxytrityl chloride

: 103024-95-9
N²-(p-anisyldiphenylmethyl)-9-<(2-hydroxyethoxy)methyl>guanine

Guidance literature:: acycloguanosine; With pyridine; chloro-trimethyl-silane; at 0 ℃; for 0.5h;

mono-4-methoxytrityl chloride; With dmap; In pyridine; at 20 ℃; for 18h;

With water; at 4 ℃; for 0.166667h;
DOI:10.1080/15257770008033022

Reference yield: 78.0%

: 103024-94-8
Acetic acid 2-(2-{[(4-methoxy-phenyl)-diphenyl-methyl]-amino}-6-oxo-1,6-dihydro-purin-9-ylmethoxy)-ethyl ester

: 103024-95-9
N²-(p-anisyldiphenylmethyl)-9-<(2-hydroxyethoxy)methyl>guanine

Guidance literature:: With ammonium hydroxide; In methanol; for 72h; Ambient temperature;
DOI:10.1021/jm00158a011

Reference yield:

: 110104-37-5
2-acetylamino-9-<(2-hydroxyethoxy)methyl>-1,9-dihydro-6H-purin-6-one

: 103024-95-9
N²-(p-anisyldiphenylmethyl)-9-<(2-hydroxyethoxy)methyl>guanine

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / triethylamine, 4-(dimethylamino)pyridine / dimethylformamide / 23 h / 50 °C

2: 78 percent / conc. NH₄OH / methanol / 72 h / Ambient temperature

With dmap; ammonium hydroxide; triethylamine; In methanol; N,N-dimethyl-formamide;
DOI:10.1021/jm00158a011