Phenol, 4-((6-(dimethylamino)-9H-purin-9-yl)methyl)-

Base Information

Chemical Name:Phenol, 4-((6-(dimethylamino)-9H-purin-9-yl)methyl)-
CAS No.:112089-08-4
Molecular Formula:C14H15 N5 O
Molecular Weight:269.306
Hs Code.:
DSSTox Substance ID:DTXSID40149866
Wikidata:Q83015737
ChEMBL ID:CHEMBL7978

Synonyms:112089-08-4;Phenol, 4-((6-(dimethylamino)-9H-purin-9-yl)methyl)-;4-[[6-(dimethylamino)purin-9-yl]methyl]phenol;Phenol, 4-[[6-(dimethylamino)-9H-purin-9-yl]methyl]-;CHEMBL7978;DTXSID40149866

Suppliers and Price of Phenol, 4-((6-(dimethylamino)-9H-purin-9-yl)methyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of Phenol, 4-((6-(dimethylamino)-9H-purin-9-yl)methyl)-

Chemical Property:

Vapor Pressure:2.14E-11mmHg at 25°C
Boiling Point:519.1°C at 760 mmHg
Flash Point:267.7°C
Density:1.32g/cm³
XLogP3:2.1
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:3
Exact Mass:269.12766012
Heavy Atom Count:20
Complexity:319

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CN(C)C1=NC=NC2=C1N=CN2CC3=CC=C(C=C3)O

Technology Process of Phenol, 4-((6-(dimethylamino)-9H-purin-9-yl)methyl)-

There total 5 articles about Phenol, 4-((6-(dimethylamino)-9H-purin-9-yl)methyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 112089-09-5
9-<4-(benzyloxy)benzyl>-6-(dimethylamino)-9H-purine

: 112089-08-4
6-(Dimethylamino)-9-(4-hydroxybenzyl)-9H-purine

Guidance literature:: With hydrogen; palladium on activated charcoal; In acetic acid; for 80h; under 1520 - 2280 Torr;
DOI:10.1021/jm00398a019

Reference yield:

: 4397-53-9
p-benzyloxybenzaldehyde

: 112089-08-4
6-(Dimethylamino)-9-(4-hydroxybenzyl)-9H-purine

Guidance literature:: Multi-step reaction with 5 steps

1: NaBH₄ / ethanol / 16 h / Ambient temperature

2: SOCl₂ / CH₂Cl₂ / 0.5 h

3: 22 percent / K₂CO₃ / dimethylformamide / 16 h / Ambient temperature

4: 63 percent / ethanol; H₂O / 15 h / Ambient temperature

5: 61 percent / hydrogen / 5percent Pd/C / acetic acid / 80 h / 1520 - 2280 Torr

With sodium tetrahydroborate; thionyl chloride; hydrogen; potassium carbonate; palladium on activated charcoal; In ethanol; dichloromethane; water; acetic acid; N,N-dimethyl-formamide;
DOI:10.1021/jm00398a019

Reference yield:

: 836-43-1
4-benzyloxybenzyl alcohol

: 112089-08-4
6-(Dimethylamino)-9-(4-hydroxybenzyl)-9H-purine

Guidance literature:: Multi-step reaction with 4 steps

1: SOCl₂ / CH₂Cl₂ / 0.5 h

2: 22 percent / K₂CO₃ / dimethylformamide / 16 h / Ambient temperature

3: 63 percent / ethanol; H₂O / 15 h / Ambient temperature

4: 61 percent / hydrogen / 5percent Pd/C / acetic acid / 80 h / 1520 - 2280 Torr

With thionyl chloride; hydrogen; potassium carbonate; palladium on activated charcoal; In ethanol; dichloromethane; water; acetic acid; N,N-dimethyl-formamide;
DOI:10.1021/jm00398a019