FMOC-D-PHENYLALANYL CHLORIDE

Base Information

Chemical Name:FMOC-D-PHENYLALANYL CHLORIDE
CAS No.:103321-58-0
Molecular Formula:C24H20ClNO3
Molecular Weight:405.881
Hs Code.:2924299090
Mol file:103321-58-0.mol

Synonyms:Fmoc-D-4-Fluorophenylalanine;Fmoc-D-phenylalanine acid chloride;fmoc-4-fluoro-phenylalanine;Fmoc-D-Phe-Cl;Fmoc-D-4-Fluorophe;Fmoc-4-fluoro-D-phenylalanine;

Suppliers and Price of FMOC-D-PHENYLALANYL CHLORIDE

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
(R)-(9H-Fluoren-9-yl)methyl(1-chloro-1-oxo-3-phenylpropan-2-yl)carbamate 97%
5g
$ 446.00

Crysdot
(R)-(9H-Fluoren-9-yl)methyl(1-chloro-1-oxo-3-phenylpropan-2-yl)carbamate 97%
1g
$ 149.00

Crysdot
(R)-(9H-Fluoren-9-yl)methyl(1-chloro-1-oxo-3-phenylpropan-2-yl)carbamate 97%
10g
$ 772.00

American Custom Chemicals Corporation
FMOC-D-PHENYLALANYL CHLORIDE 95.00%
5MG
$ 503.56

Total 7 raw suppliers

Chemical Property of FMOC-D-PHENYLALANYL CHLORIDE

Chemical Property:

Melting Point:115-117 °C
Boiling Point:596.2±50.0 °C(Predicted)
PKA:10.31±0.46(Predicted)
PSA：55.40000
Density:1.279±0.06 g/cm3(Predicted)
LogP:5.29270
Storage Temp.:Store at 0°C

Purity/Quality:

98%Min ^*data from raw suppliers

(R)-(9H-Fluoren-9-yl)methyl(1-chloro-1-oxo-3-phenylpropan-2-yl)carbamate 97% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of FMOC-D-PHENYLALANYL CHLORIDE

There total 1 articles about FMOC-D-PHENYLALANYL CHLORIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.5%

: 86123-10-6
Fmoc-D-Phe-OH

: 103321-58-0
Fmoc-D-phenylalanine acid chloride

Guidance literature:: With thionyl chloride; N,N-dimethyl-formamide; In dichloromethane; for 1h; Ambient temperature;
DOI:10.1021/jo00369a042

Reference yield: 66.0%

: 103321-58-0
Fmoc-D-phenylalanine acid chloride

: 594857-65-5
C₃₉H₄₈N₆O₅

: 594857-67-7
C₆₃H₆₇N₇O₈

Guidance literature:: With N,O-bis-(trimethylsilyl)-acetamide; In dichloromethane;
DOI:10.1016/S0960-894X(03)00412-8

Reference yield: 40.0%

: 1262307-33-4
C₇H₁₃NO₄

: 103321-58-0
Fmoc-D-phenylalanine acid chloride

: (R)-(9H-fluoren-9-yl)methyl 2-benzyl-4-((R)-3-hydroxy-1-methoxy-1-oxopropan-2-yl)-3-oxo-3,4-dihydropyrazine-1(2H)-carboxylate

Guidance literature:: C₇H₁₃NO₄; Fmoc-D-phenylalanine acid chloride; With 2,6-dimethylpyridine; In dichloromethane; at 0 - 20 ℃;

With methanesulfonic acid; In dichloromethane; toluene; for 2h; Reflux; Molecular sieve;
DOI:10.1039/c5ob00783f