Glycine, N-[2-[2-[2-[bis(carboxymethyl)amino]-5-[methoxy(3-methoxy-2,6-dinitro phenyl)methyl]phenoxy]ethoxy]-4-methylphenyl]-N-(carboxymethyl)-

Base Information

Chemical Name:Glycine, N-[2-[2-[2-[bis(carboxymethyl)amino]-5-[methoxy(3-methoxy-2,6-dinitro phenyl)methyl]phenoxy]ethoxy]-4-methylphenyl]-N-(carboxymethyl)-
CAS No.:103471-67-6
Molecular Formula:C32H34N4O16
Molecular Weight:730.639
Hs Code.:
Mol file:103471-67-6.mol

Glycine,
N-[2-[2-[2-[bis(carboxymethyl)amino]-5-[methoxy(3-methoxy-2,6-dinitro
phenyl)methyl]phenoxy]ethoxy]-4-methylphenyl]-N-(carboxymethyl)-

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Glycine, N-[2-[2-[2-[bis(carboxymethyl)amino]-5-[methoxy(3-methoxy-2,6-dinitro phenyl)methyl]phenoxy]ethoxy]-4-methylphenyl]-N-(carboxymethyl)-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Glycine, N-[2-[2-[2-[bis(carboxymethyl)amino]-5-[methoxy(3-methoxy-2,6-dinitro phenyl)methyl]phenoxy]ethoxy]-4-methylphenyl]-N-(carboxymethyl)-

There total 3 articles about Glycine, N-[2-[2-[2-[bis(carboxymethyl)amino]-5-[methoxy(3-methoxy-2,6-dinitro phenyl)methyl]phenoxy]ethoxy]-4-methylphenyl]-N-(carboxymethyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 103471-66-5
({2-{2-[2-(Bis-methoxycarbonylmethyl-amino)-5-methyl-phenoxy]-ethoxy}-4-[methoxy-(3-methoxy-2,6-dinitro-phenyl)-methyl]-phenyl}-methoxycarbonylmethyl-amino)-acetic acid methyl ester

: 103471-67-6
({2-{2-[2-(Bis-carboxymethyl-amino)-5-methyl-phenoxy]-ethoxy}-4-[methoxy-(3-methoxy-2,6-dinitro-phenyl)-methyl]-phenyl}-carboxymethyl-amino)-acetic acid

Guidance literature:: With potassium hydroxide; In 1,4-dioxane; methanol; water;
DOI:10.1021/ja00218a034

Reference yield:

: 103471-65-4
2,6-dinitro-3-methoxybenzaldehyde dimethyl acetal

: 103471-67-6
({2-{2-[2-(Bis-carboxymethyl-amino)-5-methyl-phenoxy]-ethoxy}-4-[methoxy-(3-methoxy-2,6-dinitro-phenyl)-methyl]-phenyl}-carboxymethyl-amino)-acetic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) trimethylsilyl trifluoromethanesulfonate, 2,6-di-tert-butylpyridine; 2.) tetrabutylammonium fluoride trihydrate / 1.) CHCl₃, room temp.; 2.) CHCl₃, room temp., 15 min.

2: 1M KOH then acid / dioxane; methanol; H₂O

With potassium hydroxide; 2,6-di-tert-butyl-pyridine; trimethylsilyl trifluoromethanesulfonate; tetrabutyl ammonium fluoride; In 1,4-dioxane; methanol; water;
DOI:10.1021/ja00218a034

Reference yield:

: 96315-10-5
N-(2-(2-(2-(bis(methoxycarbonylmethyl)amino)phenoxy)ethoxy)-4-methylphenyl)-N-(methoxycarbonylmethyl)aminoacetic acid methyl ester

: 103471-67-6
({2-{2-[2-(Bis-carboxymethyl-amino)-5-methyl-phenoxy]-ethoxy}-4-[methoxy-(3-methoxy-2,6-dinitro-phenyl)-methyl]-phenyl}-carboxymethyl-amino)-acetic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) trimethylsilyl trifluoromethanesulfonate, 2,6-di-tert-butylpyridine; 2.) tetrabutylammonium fluoride trihydrate / 1.) CHCl₃, room temp.; 2.) CHCl₃, room temp., 15 min.

2: 1M KOH then acid / dioxane; methanol; H₂O

With potassium hydroxide; 2,6-di-tert-butyl-pyridine; trimethylsilyl trifluoromethanesulfonate; tetrabutyl ammonium fluoride; In 1,4-dioxane; methanol; water;
DOI:10.1021/ja00218a034