3-(Benzenesulfonyl)-4-hydroxy-2-methylidene-N-phenyldodecanamide

Base Information

Chemical Name:3-(Benzenesulfonyl)-4-hydroxy-2-methylidene-N-phenyldodecanamide
CAS No.:103633-59-6
Molecular Formula:C25H33NO4S
Molecular Weight:443.607
Hs Code.:
DSSTox Substance ID:DTXSID30542908
Mol file:103633-59-6.mol

Synonyms:103633-59-6;DTXSID30542908;3-(BENZENESULFONYL)-4-HYDROXY-2-METHYLIDENE-N-PHENYLDODECANAMIDE

Suppliers and Price of 3-(Benzenesulfonyl)-4-hydroxy-2-methylidene-N-phenyldodecanamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 0 raw suppliers

Chemical Property of 3-(Benzenesulfonyl)-4-hydroxy-2-methylidene-N-phenyldodecanamide

Chemical Property:

XLogP3:5.8
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:13
Exact Mass:443.21302971
Heavy Atom Count:31
Complexity:643

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCCCCCCCC(C(C(=C)C(=O)NC1=CC=CC=C1)S(=O)(=O)C2=CC=CC=C2)O

Technology Process of 3-(Benzenesulfonyl)-4-hydroxy-2-methylidene-N-phenyldodecanamide

There total 4 articles about 3-(Benzenesulfonyl)-4-hydroxy-2-methylidene-N-phenyldodecanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 124-19-6
nonan-1-al

: C₁₆H₁₃NO^(2-)*2Li⁽¹⁺⁾

: 103633-59-6
4-hydroxy-2-methylene-N-phenyl-3-(phenylsulfonyl)dodecanamide

Guidance literature:: In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; at -78 ℃; for 2h;
DOI:10.1016/S0040-4039(00)94941-4

Reference yield:

: 99699-32-8
2-methylene-N-phenyl-2-[(tributylstannyl)methyl]propanamide

: 103633-59-6
4-hydroxy-2-methylene-N-phenyl-3-(phenylsulfonyl)dodecanamide

Guidance literature:: Multi-step reaction with 3 steps

1: 89 percent / iodine

2: butyllithium / tetrahydrofuran; hexamethylphosphoric acid triamide / 0.5 h / -78 °C

With n-butyllithium; iodine; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide;
DOI:10.1016/S0040-4039(00)94940-2

Reference yield:

: 87504-85-6
N-phenyl-2-<(phenylsulfonyl)methyl>propenamide

: 103633-59-6
4-hydroxy-2-methylene-N-phenyl-3-(phenylsulfonyl)dodecanamide

Guidance literature:: Multi-step reaction with 2 steps

1: butyllithium / tetrahydrofuran; hexamethylphosphoric acid triamide / 0.5 h / -78 °C

With n-butyllithium; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide;
DOI:10.1016/S0040-4039(00)94940-2