Carbamic acid, [5-[[(4-methylphenyl)sulfonyl]amino]-6-[(4-nitrophenyl)amino]-6-oxohexyl] -, phenylmethyl ester, (S)-

Base Information

• Chemical Name: Carbamic acid, [5-[[(4-methylphenyl)sulfonyl]amino]-6-[(4-nitrophenyl)amino]-6-oxohexyl] -, phenylmethyl ester, (S)-
• CAS No.: 103892-79-1
• Molecular Formula: C27H30N4O7S
• Molecular Weight: 554.624
• Mol file: 103892-79-1.mol

Synonyms:

Chemical Property of Carbamic acid, [5-[[(4-methylphenyl)sulfonyl]amino]-6-[(4-nitrophenyl)amino]-6-oxohexyl] -, phenylmethyl ester, (S)-

Chemical Property:

Purity/Quality:

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MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Carbamic acid, [5-[[(4-methylphenyl)sulfonyl]amino]-6-[(4-nitrophenyl)amino]-6-oxohexyl] -, phenylmethyl ester, (S)-

There total 1 articles about Carbamic acid, [5-[[(4-methylphenyl)sulfonyl]amino]-6-[(4-nitrophenyl)amino]-6-oxohexyl] -, phenylmethyl ester, (S)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

N-tosyl-N'-benzyloxycarbonyl-L-lysine (34235-82-0) + 4-nitro-aniline (100-01-6,104810-17-5) → [(S)-5-(4-Nitro-phenylcarbamoyl)-5-(toluene-4-sulfonylamino)-pentyl]-carbamic acid benzyl ester (103892-79-1)

Guidance literature:

With phosphorus trichloride; In pyridine; 1.) 15 min, -15 deg C; 2.) 3 h, 60 deg C;

DOI:10.1248/cpb.36.1289

Reference yield: 39.0%

[(S)-5-(4-Nitro-phenylcarbamoyl)-5-(toluene-4-sulfonylamino)-pentyl]-carbamic acid benzyl ester (103892-79-1) → (S)-6-Amino-2-(toluene-4-sulfonylamino)-hexanoic acid (4-nitro-phenyl)-amide; hydrochloride (103892-20-2)

Guidance literature:

With hydrogen bromide; acetic acid; 1.) 0 deg C, 5 min.; 2.) r.t., 50 min.;

DOI:10.1248/cpb.36.1289

upstream raw materials:

N-tosyl-N'-benzyloxycarbonyl-L-lysine

4-nitro-aniline

Downstream raw materials:

(S)-6-Amino-2-(toluene-4-sulfonylamino)-hexanoic acid (4-nitro-phenyl)-amide; hydrochloride

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