Acetic acid, (3,5-dimethylphenoxy)-, 2-[(phenylamino)thioxomethyl]hydrazide

Base Information

• Chemical Name: Acetic acid, (3,5-dimethylphenoxy)-, 2-[(phenylamino)thioxomethyl]hydrazide
• CAS No.: 103896-76-0
• Molecular Formula: C₁₇H₁₉N₃O₂S
• Molecular Weight: 329.423
• Mol file: 103896-76-0.mol

Synonyms:

Chemical Property of Acetic acid, (3,5-dimethylphenoxy)-, 2-[(phenylamino)thioxomethyl]hydrazide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Acetic acid, (3,5-dimethylphenoxy)-, 2-[(phenylamino)thioxomethyl]hydrazide

There total 3 articles about Acetic acid, (3,5-dimethylphenoxy)-, 2-[(phenylamino)thioxomethyl]hydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

2-(3,5-dimethylphenoxy)acetohydrazide (83798-15-6) + phenyl isothiocyanate (103-72-0) → C17H19N3O2S (103896-76-0)

Guidance literature:

In methanol; Heating;

Reference yield:

ethyl 2-(3,5-dimethylphenoxy)acetate (24242-74-8) → C17H19N3O2S (103896-76-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 68 percent / hydrazine hydrate / ethanol / 12 h / Heating

2: benzene / Heating

With hydrazine hydrate; In ethanol; benzene;

Reference yield:

3,5-Dimethylphenol (108-68-9,50356-23-5) → C17H19N3O2S (103896-76-0)

Guidance literature:

Multi-step reaction with 3 steps

1: K₂CO₃ / acetone / 15 h / Heating

2: 68 percent / hydrazine hydrate / ethanol / 12 h / Heating

3: benzene / Heating

With potassium carbonate; hydrazine hydrate; In ethanol; acetone; benzene;

upstream raw materials:

2-(3,5-dimethylphenoxy)acetohydrazide

phenyl isothiocyanate

ethyl 2-(3,5-dimethylphenoxy)acetate

3,5-Dimethylphenol

Downstream raw materials:

[5-(3,5-Dimethyl-phenoxymethyl)-4-phenyl-4H-[1,2,4]triazol-3-ylsulfanyl]-acetic acid

2-(3,5-Dimethyl-phenoxy)-N-{4-oxo-2-[(Z)-phenylimino]-thiazolidin-3-yl}-acetamide

5-(3,5-dimethylphenoxymethyl)-4-phenyl-s-triazole-3-thiol

Refernces

• 1、 Khan, R. H.,Srivastava, R. A. K.,Rastogi, R. C.. "Synthesis and Antifungal and Antibacterial Activities of Some New 4-Aryl-5-aryloxymethyl-1,2,4-triazole-3-thiols and Their 3-Mercaptoacetic Acids". . p. 883 - 885. Retrieved 2007/10/02.