Benzenesulfonamide, 4-methyl-N-(tetrahydro-2-oxo-3-furanyl)-, (S)-

Base Information

Chemical Name:Benzenesulfonamide, 4-methyl-N-(tetrahydro-2-oxo-3-furanyl)-, (S)-
CAS No.:10396-97-1
Molecular Formula:C11H13NO4S
Molecular Weight:255.295
Hs Code.:
Mol file:10396-97-1.mol

Synonyms:N-p-toluenesulfonyl-L-homoserine lactone;(S)-N-tosylhomoserine γ-lactone;N-tosylhomoserine lactone;4-methyl-N-((S)-2-oxotetrahydrofuran-3-yl)benzenesulfonamide;4-Methyl-N-((S)-2-oxo-tetrahydro-furan-3-yl)-benzenesulfonamide;L-N-tosyl-α-amino-γ-butyrolactone;

Suppliers and Price of Benzenesulfonamide, 4-methyl-N-(tetrahydro-2-oxo-3-furanyl)-, (S)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Benzenesulfonamide, 4-methyl-N-(tetrahydro-2-oxo-3-furanyl)-, (S)-

Chemical Property:

Melting Point:136-138 °C
Boiling Point:471.6±55.0 °C(Predicted)
PSA：80.85000
Density:1.38±0.1 g/cm3(Predicted)
LogP:2.06050

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Benzenesulfonamide, 4-methyl-N-(tetrahydro-2-oxo-3-furanyl)-, (S)-

There total 6 articles about Benzenesulfonamide, 4-methyl-N-(tetrahydro-2-oxo-3-furanyl)-, (S)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 6305-38-0,15295-77-9,67580-93-2,110045-70-0
(S)-(-)-α-amino-γ-butyrolactone hydrobromide

: 98-59-9
p-toluenesulfonyl chloride

: 10396-97-1
4-methyl-N-((S)-2-oxotetrahydrofuran-3-yl)benzenesulfonamide

Guidance literature:: With triethylamine; In tetrahydrofuran; at 0 - 20 ℃; for 12h;
DOI:10.1002/chem.201500886

Reference yield:

: 143947-81-3
[(S)-5-Oxo-3-(toluene-4-sulfonyl)-oxazolidin-4-yl]-acetaldehyde

: 10396-97-1
4-methyl-N-((S)-2-oxotetrahydrofuran-3-yl)benzenesulfonamide

Guidance literature:: With hydrogen; tris(triphenylphosphine)ruthenium(II) chloride; In benzene; under 7600 Torr;
DOI:10.1016/S0040-4039(00)79053-8

Reference yield:

: C₁₇H₂₁NO₈S

: 10396-97-1
4-methyl-N-((S)-2-oxotetrahydrofuran-3-yl)benzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: sodium tetrahydroborate / tetrahydrofuran

2: citric acid / 2 h / Reflux

With sodium tetrahydroborate; citric acid; In tetrahydrofuran;
DOI:10.1021/jo2008093