2-Methyl-2-butenoic acid 2,3,3a,4,5,6,7,8,9,11a-decahydro-7,9-dihydroxy-6,10-dimethyl-3-methylene-2-oxo-6,9-epoxycyclodeca[b]furan-4-yl ester

Base Information

• Chemical Name: 2-Methyl-2-butenoic acid 2,3,3a,4,5,6,7,8,9,11a-decahydro-7,9-dihydroxy-6,10-dimethyl-3-methylene-2-oxo-6,9-epoxycyclodeca[b]furan-4-yl ester
• CAS No.: 80482-71-9
• Molecular Formula: C₂₀H₂₆O₇
• Molecular Weight: 378.422
• Mol file: 80482-71-9.mol

Synonyms:

Chemical Property of 2-Methyl-2-butenoic acid 2,3,3a,4,5,6,7,8,9,11a-decahydro-7,9-dihydroxy-6,10-dimethyl-3-methylene-2-oxo-6,9-epoxycyclodeca[b]furan-4-yl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-Methyl-2-butenoic acid 2,3,3a,4,5,6,7,8,9,11a-decahydro-7,9-dihydroxy-6,10-dimethyl-3-methylene-2-oxo-6,9-epoxycyclodeca[b]furan-4-yl ester

There total 1 articles about 2-Methyl-2-butenoic acid 2,3,3a,4,5,6,7,8,9,11a-decahydro-7,9-dihydroxy-6,10-dimethyl-3-methylene-2-oxo-6,9-epoxycyclodeca[b]furan-4-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(Z)-2-Methyl-but-2-enoic acid (Z)-(4S,9R,11R,12S)-12-hydroxy-2,11-dimethyl-7-methylene-6-oxo-5,14-dioxa-tricyclo[9.2.1.04,8]tetradec-2-en-9-yl ester (78657-58-6) → (Z)-2-Methyl-but-2-enoic acid (Z)-(1R,4S,9R,11R,12S)-1,12-dihydroxy-2,11-dimethyl-7-methylene-6-oxo-5,14-dioxa-tricyclo[9.2.1.04,8]tetradec-2-en-9-yl ester (80482-71-9) + (Z)-2-Methyl-but-2-enoic acid (Z)-(4R,6R,9S,11aS)-6,9-dihydroxy-6,10-dimethyl-3-methylene-2,7-dioxo-2,3,3a,4,5,6,7,8,9,11a-decahydro-cyclodeca[b]furan-4-yl ester + C20H22O7 + (Z)-2-Methyl-but-2-enoic acid (Z)-(4S,9R,11R)-2,11-dimethyl-7-methylene-6,12-dioxo-5,14-dioxa-tricyclo[9.2.1.04,8]tetradeca-1(13),2-dien-9-yl ester

Guidance literature:

With jones' reagent; In acetone; at 0 ℃; for 1h;

DOI:10.1016/0031-9422(81)85224-7

Reference yield:

(Z)-2-Methyl-but-2-enoic acid (Z)-(1R,4S,9R,11R,12S)-1,12-dihydroxy-2,11-dimethyl-7-methylene-6-oxo-5,14-dioxa-tricyclo[9.2.1.04,8]tetradec-2-en-9-yl ester (80482-71-9) → (Z)-2-Methyl-but-2-enoic acid (Z)-(4S,9R,11R)-2,11-dimethyl-7-methylene-6,12-dioxo-5,14-dioxa-tricyclo[9.2.1.04,8]tetradeca-1(13),2-dien-9-yl ester

Guidance literature:

With jones' reagent; for 1h; Ambient temperature;

DOI:10.1016/0031-9422(81)85224-7

upstream raw materials:

(Z)-2-Methyl-but-2-enoic acid (Z)-(4S,9R,11R,12S)-12-hydroxy-2,11-dimethyl-7-methylene-6-oxo-5,14-dioxa-tricyclo[9.2.1.0^4,8]tetradec-2-en-9-yl ester