1-Dec-1-en-2-ylsulfonyl-4-methylbenzene

Base Information

Chemical Name:1-Dec-1-en-2-ylsulfonyl-4-methylbenzene
CAS No.:105235-54-9
Molecular Formula:C17H26O2S
Molecular Weight:294.458
Hs Code.:
DSSTox Substance ID:DTXSID00544378
Wikidata:Q82421481
Mol file:105235-54-9.mol

Synonyms:1-dec-1-en-2-ylsulfonyl-4-methylbenzene;105235-54-9;DTXSID00544378;1-methyl-4-[(1-octylvinyl)sulfonyl]benzene;1-(DEC-1-ENE-2-SULFONYL)-4-METHYLBENZENE

Suppliers and Price of 1-Dec-1-en-2-ylsulfonyl-4-methylbenzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-Dec-1-en-2-ylsulfonyl-4-methylbenzene

Chemical Property:

XLogP3:5.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:9
Exact Mass:294.16535124
Heavy Atom Count:20
Complexity:370

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCCCCCCCC(=C)S(=O)(=O)C1=CC=C(C=C1)C

Technology Process of 1-Dec-1-en-2-ylsulfonyl-4-methylbenzene

There total 5 articles about 1-Dec-1-en-2-ylsulfonyl-4-methylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 105465-46-1
1-[2-(Toluene-4-sulfonyl)-decyl]-pyrrolidine

: 105235-54-9
2-tosyl-1-decene

Guidance literature:: With sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; for 24h; Ambient temperature;
DOI:10.1246/cl.1986.341

Reference yield:

: 16191-66-5
1-[2-(toluene-4-sulfonyl)-ethyl]-pyrrolidine

: 105235-54-9
2-tosyl-1-decene

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) butyllithium (BuLi), HMPA / 1.)THF, hexane, -72 deg C, 30 min; 2.) THF, -72 deg C, 1 h

2: 95 percent / m-chloroperbenzoic acid (MCPBA), sodium hydrocarbonate (NaHCO₃) / CH₂Cl₂ / 24 h / Ambient temperature

With N,N,N,N,N,N-hexamethylphosphoric triamide; n-butyllithium; sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; In dichloromethane;
DOI:10.1246/cl.1986.341

Reference yield:

: 5535-52-4
tolyl vinyl sulfone

: 105235-54-9
2-tosyl-1-decene

Guidance literature:: Multi-step reaction with 3 steps

1: 253 mg / acetonitrile / 28 h / Ambient temperature

2: 1.) butyllithium (BuLi), HMPA / 1.)THF, hexane, -72 deg C, 30 min; 2.) THF, -72 deg C, 1 h

3: 95 percent / m-chloroperbenzoic acid (MCPBA), sodium hydrocarbonate (NaHCO₃) / CH₂Cl₂ / 24 h / Ambient temperature

With N,N,N,N,N,N-hexamethylphosphoric triamide; n-butyllithium; sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; acetonitrile;
DOI:10.1246/cl.1986.341