Acetamide, N-(4-azidophenyl)-2-diazo-

Base Information

Chemical Name:Acetamide, N-(4-azidophenyl)-2-diazo-
CAS No.:105311-00-0
Molecular Formula:C8H6N6O
Molecular Weight:202.175
Hs Code.:

Synonyms:

Suppliers and Price of Acetamide, N-(4-azidophenyl)-2-diazo-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Acetamide, N-(4-azidophenyl)-2-diazo-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Acetamide, N-(4-azidophenyl)-2-diazo-

There total 6 articles about Acetamide, N-(4-azidophenyl)-2-diazo- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: N-(4-azidophenyl)-α-aminoacetamide hydrochloride

: 105311-00-0
N-(4-azidophenyl)-α-diazoacetamide

Guidance literature:: With acetic acid; sodium nitrite; In tetrahydrofuran; water; ethyl acetate; for 1.5h;
DOI:10.1021/jo00376a057

Reference yield:

: 100-01-6,104810-17-5
4-nitro-aniline

: 105311-00-0
N-(4-azidophenyl)-α-diazoacetamide

Guidance literature:: Multi-step reaction with 5 steps

1: 33 percent / 1,3-dicyclohexylcarbodiimide / tetrahydrofuran / 18 h / 25 °C

2: 38 percent / iron, glacial acetic acid / acetone; H₂O / 5 h / Heating

3: 1.) sodium nitrite, HCl, 2.) sodium azide / 1.) THF, water, 0-5 deg C, 30 min, 2.) THF, water, 30 min

4: 80 percent / HCl, glacial acetic acid / 0.5 h / 25 °C

5: 69 percent / sodium nitrite, glacial acetic acid / H₂O; tetrahydrofuran; ethyl acetate / 1.5 h

With hydrogenchloride; sodium azide; iron; acetic acid; dicyclohexyl-carbodiimide; sodium nitrite; In tetrahydrofuran; water; ethyl acetate; acetone;
DOI:10.1021/jo00376a057

Reference yield:

: 83209-85-2
N-(4-aminophenyl)-α-<(tert-butoxycarbonyl)amino>acetamide

: 105311-00-0
N-(4-azidophenyl)-α-diazoacetamide

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) sodium nitrite, HCl, 2.) sodium azide / 1.) THF, water, 0-5 deg C, 30 min, 2.) THF, water, 30 min

2: 80 percent / HCl, glacial acetic acid / 0.5 h / 25 °C

3: 69 percent / sodium nitrite, glacial acetic acid / H₂O; tetrahydrofuran; ethyl acetate / 1.5 h

With hydrogenchloride; sodium azide; acetic acid; sodium nitrite; In tetrahydrofuran; water; ethyl acetate;
DOI:10.1021/jo00376a057