DIISOPROPYLSULFAMOYL CHLORIDE

Base Information

• Chemical Name: DIISOPROPYLSULFAMOYL CHLORIDE
• CAS No.: 10539-95-4
• Molecular Formula: C6H14ClNO2S
• Molecular Weight: 199.702
• Hs Code.: 2935009090
• Mol file: 10539-95-4.mol

Synonyms:Chlor-N,N-diisopropylsulfonamid;Chlormethylsulfonyl-pyrrolidin;1-[(CHLOROMETHYL)SULFONYL]PYRROLIDINE;Pyrrolidine,1-(chloromethylsulfonyl);

Chemical Property of DIISOPROPYLSULFAMOYL CHLORIDE

Chemical Property:

• Vapor Pressure: 0.027mmHg at 25°C
• Boiling Point: 246.642oC at 760 mmHg
• PKA: -9.24±0.70(Predicted)
• Flash Point: 102.966oC
• PSA: 45.76000
• Density: 1.189g/cm3
• LogP: 2.66960

Purity/Quality:

98%,99%, ^*data from raw suppliers

Diisopropylsulfamoylchloride ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of DIISOPROPYLSULFAMOYL CHLORIDE

There total 1 articles about DIISOPROPYLSULFAMOYL CHLORIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 14.0%

diisopropylamine (108-18-9) → Chlor-N,N-diisopropylsulfonamid (10539-95-4)

Guidance literature:

With sulfuryl dichloride; In ethylene glycol; at -15 - 20 ℃; for 3.83333h;

DOI:10.1055/a-1548-8362

Reference yield: 49.0%

Chlor-N,N-diisopropylsulfonamid (10539-95-4) + (S,S)-1,2-diphenyl-1,2-diaminoethane (29841-69-8) → (1S,2S)-N-(N,N-diisopropylsulfamoyl)-1,2-diphenylethylenediamine

Guidance literature:

In dichloromethane; at 0 - 20 ℃;

DOI:10.1016/S0957-4166(02)00659-6

Reference yield: 16.0%

Chlor-N,N-diisopropylsulfonamid (10539-95-4) + N-acetyl-N'-(4-hydroxyphenyl)piperazine (67914-60-7,89929-31-7) → 4-(4-acetylpiperazin-1-yl)phenyl diisopropylsulfamate

Guidance literature:

N-acetyl-N'-(4-hydroxyphenyl)piperazine; With sodium hydride; In 1,2-dimethoxyethane; at 0 - 20 ℃; for 0.166667h;

Chlor-N,N-diisopropylsulfonamid; In 1,2-dimethoxyethane; at 0 - 20 ℃; for 15h;

DOI:10.1055/a-1548-8362

upstream raw materials:

diisopropylamine