Benzenamine, N-hydroxy-N-nitroso-4-octadecyl-, ammonium salt

Base Information

• Chemical Name: Benzenamine, N-hydroxy-N-nitroso-4-octadecyl-, ammonium salt
• CAS No.: 105772-51-8
• Molecular Formula: C₂₄H₄₂N₂O₂*H₃N
• Molecular Weight: 407.64
• Mol file: 105772-51-8.mol

Synonyms:

Chemical Property of Benzenamine, N-hydroxy-N-nitroso-4-octadecyl-, ammonium salt

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Benzenamine, N-hydroxy-N-nitroso-4-octadecyl-, ammonium salt

There total 2 articles about Benzenamine, N-hydroxy-N-nitroso-4-octadecyl-, ammonium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-(4-Octadecyl-phenyl)-hydroxylamine (127290-48-6) → N-nitroso-N-p-octadecylphenylhydroxylamine ammonium salt (105772-51-8)

Guidance literature:

With n-Butyl nitrite; ammonia; In diethyl ether; at 15 ℃; for 0.5h;

DOI:10.1246/bcsj.63.920

Reference yield:

p-nitrooctadecylbenzene (127274-77-5) → N-nitroso-N-p-octadecylphenylhydroxylamine ammonium salt (105772-51-8)

Guidance literature:

Multi-step reaction with 2 steps

1: Zn powder, NH₄Cl / 1 h / 70 °C

2: NH₃, n-C₄H₉ONO / diethyl ether / 0.5 h / 15 °C

With n-Butyl nitrite; ammonia; ammonium chloride; zinc; In diethyl ether;

DOI:10.1246/bcsj.63.920

upstream raw materials:

N-(4-Octadecyl-phenyl)-hydroxylamine

p-nitrooctadecylbenzene

Refernces