1-(4-fluorophenyl)-2,3,4,9-tetrahydro-1H-beta-carboline hydrochloride (1:1)

Base Information

• Chemical Name: 1-(4-fluorophenyl)-2,3,4,9-tetrahydro-1H-beta-carboline hydrochloride (1:1)
• CAS No.: 3380-82-3
• Molecular Formula: C17H16ClFN2
• Molecular Weight: 302.7737

Synonyms:

Chemical Property of 1-(4-fluorophenyl)-2,3,4,9-tetrahydro-1H-beta-carboline hydrochloride (1:1)

Chemical Property:

• Vapor Pressure: 5.3E-08mmHg at 25°C
• Boiling Point: 441.8°C at 760 mmHg
• Flash Point: 221°C

Purity/Quality:

95% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-(4-fluorophenyl)-2,3,4,9-tetrahydro-1H-beta-carboline hydrochloride (1:1)

There total 1 articles about 1-(4-fluorophenyl)-2,3,4,9-tetrahydro-1H-beta-carboline hydrochloride (1:1) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

tryptamine hydochloride (343-94-2) + 4-fluorobenzaldehyde (459-57-4) → rac-1-(4-fluorophenyl)-2,3,4,9-tetrahydro-1H-pyrido[3,4-b]indole hydrochloride (3380-82-3)

Guidance literature:

for 0.0416667h; microwave irradiation;

DOI:10.1080/00397910701572555

Reference yield:

rac-1-(4-fluorophenyl)-2,3,4,9-tetrahydro-1H-pyrido[3,4-b]indole hydrochloride (3380-82-3) → 1-(4-fluorophenyl)-2,3,4,9-tetrahydro-1H-pyrido[3,4-b]indole (221620-96-8)

Guidance literature:

With sodium carbonate; In water;

DOI:10.1002/chem.202004449

upstream raw materials:

tryptamine hydochloride

4-fluorobenzaldehyde

Downstream raw materials:

1-(4-fluorophenyl)-2,3,4,9-tetrahydro-1H-pyrido[3,4-b]indole

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