4-BROMOPHTHALIC ACID MONOSODIUM SALT

Base Information

• Chemical Name: 4-BROMOPHTHALIC ACID MONOSODIUM SALT
• CAS No.: 106701-82-0
• Molecular Formula: C8H5BrO4.Na
• Molecular Weight: 267.011
• Mol file: 106701-82-0.mol

Synonyms:monosodium 4-bromophthalate;4-BROMOPHTHALIC ACID MONOSODIUM SALT;

Chemical Property of 4-BROMOPHTHALIC ACID MONOSODIUM SALT

Chemical Property:

• PSA: 77.43000
• LogP: 0.51080

Purity/Quality:

4-BROMOPHTHALIC ACID MONOSODIUM SALT 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-BROMOPHTHALIC ACID MONOSODIUM SALT

There total 1 articles about 4-BROMOPHTHALIC ACID MONOSODIUM SALT which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 22.0%

phthalic anhydride (85-44-9) → 4-bromophthalic acid monosodium salt (106701-82-0)

Guidance literature:

With bromine; sodium hydroxide; In water; at 90 ℃; for 7h;

DOI:10.1002/pola.26485

Reference yield: 96.0%

4-bromophthalic acid monosodium salt (106701-82-0) + isopropyl alcohol (67-63-0,8013-70-5) → di(isopropyl) 4-bromophthalate (1431380-27-6)

Guidance literature:

With thionyl chloride; for 2h; Reflux;

DOI:10.1002/pola.26485

Reference yield: 95.0%

4-bromophthalic acid monosodium salt (106701-82-0) + phenylacetylene (536-74-3) → 4-phenylethynylphthalic acid

Guidance literature:

4-bromophthalic acid monosodium salt; With tetrabutylammomium bromide; trisodium tris(3-sulfophenyl)phosphine; palladium diacetate; sodium hydroxide; In water; at 60 ℃; for 0.5h; Inert atmosphere;

phenylacetylene; In water; for 3h; Inert atmosphere; Reflux;

DOI:10.3184/174751912X13366326240908

upstream raw materials:

phthalic anhydride

Downstream raw materials:

di(iso-butyl) 4-vinylphthalate

di(2-ethyl-1-hexyl) 4-vinylphthalate

4-bromophthalic acid

diethyl 4-vinylphthalate