15,16-Diazatricyclo[9.3.1.14,8]hexadeca-1(15),4,6,8(16),11,13-hexaene

Base Information

Chemical Name:15,16-Diazatricyclo[9.3.1.14,8]hexadeca-1(15),4,6,8(16),11,13-hexaene
CAS No.:6574-83-0
Molecular Formula:C14H14N2
Molecular Weight:210.27
Hs Code.:

Synonyms:1,4(2,6)-dipyridina-cyclohexaphane;1,4-Di-(2,6)pyrida-cyclohexan;<2.2>(2,6)Pyridinophan;15,16-Diaza-tricyclo[9.3.1.14,8]hexadeca-1(14),4,6,8(16),11(15),12-hexaene;<2,2>(2,6)Pyridinophan;15,16-diaza-tricyclo[9.3.1.14,8]hexadeca-1(15),4,6,8(16),11,13-hexaene;

Suppliers and Price of 15,16-Diazatricyclo[9.3.1.14,8]hexadeca-1(15),4,6,8(16),11,13-hexaene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 3 raw suppliers

Chemical Property of 15,16-Diazatricyclo[9.3.1.14,8]hexadeca-1(15),4,6,8(16),11,13-hexaene

Chemical Property:

Vapor Pressure:0.000967mmHg at 25°C
Boiling Point:312.5°C at 760 mmHg
Flash Point:118°C
PSA：25.78000
Density:1.118g/cm³
LogP:2.36040

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 15,16-Diazatricyclo[9.3.1.14,8]hexadeca-1(15),4,6,8(16),11,13-hexaene

There total 15 articles about 15,16-Diazatricyclo[9.3.1.14,8]hexadeca-1(15),4,6,8(16),11,13-hexaene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 117655-05-7
3,11-Dinitroso-3,11,17,18-tetraaza-tricyclo[11.3.1.1^5,9]octadeca-1⁽¹⁶⁾,5,7,9⁽¹⁸⁾,13⁽¹⁷⁾,14-hexaene

: 6574-83-0
anti-4,12-diaza<2₂>(1,3)cyclophane

Guidance literature:: With potassium hydroxide; sodium disulfite; In ethanol; water; Heating;
DOI:10.1016/0040-4039(88)85327-9

Reference yield: 9.0%

: 7703-74-4
2,6-bis-(bromomethyl)pyridine

: 6574-83-0
anti-4,12-diaza<2₂>(1,3)cyclophane

Guidance literature:: With cesium hydroxide; phenyllithium; In 1,4-dioxane; diethyl ether; benzene; 1.) 2 h, room temp.; 2.) 15 h, reflux;

Reference yield:

: 115078-43-8
3,11,17,18-tetraazatricyclo<11.3.1.1^5,9>octadeca-1(17),5(18),6,8,13,15-hexaene

: 6574-83-0
anti-4,12-diaza<2₂>(1,3)cyclophane

Guidance literature:: Multi-step reaction with 2 steps

1: NaNO₂, conc. aq. HCl / H₂O / Ambient temperature

2: 85 percent / KOH, sodium hydrosulfite / H₂O; ethanol / Heating

With hydrogenchloride; potassium hydroxide; sodium disulfite; sodium nitrite; In ethanol; water;
DOI:10.1016/0040-4039(88)85327-9