2-(methylsulfonyl)-3-phenyloxaziridine

Base Information

Chemical Name:2-(methylsulfonyl)-3-phenyloxaziridine
CAS No.:73844-99-2
Molecular Formula:C8H9NO3S
Molecular Weight:199.23
Hs Code.:

Synonyms:

Suppliers and Price of 2-(methylsulfonyl)-3-phenyloxaziridine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 2-(methylsulfonyl)-3-phenyloxaziridine

Chemical Property:

Vapor Pressure:0.00109mmHg at 25°C
Boiling Point:300.8°C at 760 mmHg
Flash Point:135.7°C
Density:1.44g/cm³

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-(methylsulfonyl)-3-phenyloxaziridine

There total 5 articles about 2-(methylsulfonyl)-3-phenyloxaziridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 73845-05-3,108440-09-1,14674-34-1
N-methanesulfonyl benzylideneamine

: 73844-99-2
(2R,3R)-2-Methanesulfonyl-3-phenyl-oxaziridine

Guidance literature:: With sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; N-benzyl-N,N,N-triethylammonium chloride; In chloroform; water; at 0 - 5 ℃; for 0.25h;
DOI:10.1021/jo00348a039

Reference yield:

: 774-48-1
(diethoxymethyl)benzene

: 73844-99-2
(2R,3R)-2-Methanesulfonyl-3-phenyl-oxaziridine

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / 0.5 h / 150 - 180 °C

2: 64 percent / NaHCO₃, m-chloroperbenzoic acid / CHCl₃; H₂O / 4 h / m-chloroperbenzoic acid was added at 0 deg C over 45 min

With sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; In chloroform; water;
DOI:10.1021/ja00526a040

Reference yield:

: 73845-05-3,108440-09-1,14674-34-1
N-methanesulfonyl benzylideneamine

: 73844-99-2,85653-70-9,112789-83-0
2-Methanesulfonyl-3-phenyl-oxaziridine

: 73844-99-2,85653-70-9,112789-83-0
2-Methanesulfonyl-3-phenyl-oxaziridine

Guidance literature:: With potassium hydroxide; (1S)-(+)-peroxycamphoric acid; In methanol; dichloromethane; at -60 ℃; for 3h; Yield given; pH 9-10;
DOI:10.1016/S0040-4020(01)97646-X