Benzoic acid, 4-methoxy-, (1,2-dimethyl-1,2-ethanediylidene)dihydrazide

Base Information

• Chemical Name: Benzoic acid, 4-methoxy-, (1,2-dimethyl-1,2-ethanediylidene)dihydrazide
• CAS No.: 107811-53-0
• Molecular Formula: C20H22N4O4
• Molecular Weight: 382.419
• Mol file: 107811-53-0.mol

Synonyms:

Chemical Property of Benzoic acid, 4-methoxy-, (1,2-dimethyl-1,2-ethanediylidene)dihydrazide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Benzoic acid, 4-methoxy-, (1,2-dimethyl-1,2-ethanediylidene)dihydrazide

There total 1 articles about Benzoic acid, 4-methoxy-, (1,2-dimethyl-1,2-ethanediylidene)dihydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

4-methoxybenzoic acid hydrazide (3290-99-1) + dimethylglyoxal (431-03-8) → 2,3-butanedione bis(4-methoxybenzoylhydrazone) (107811-53-0)

Guidance literature:

In ethanol; for 4h; Ambient temperature;

Reference yield: 90.0%

uranyl(VI) acetate dihydrate + 2,3-butanedione bis(4-methoxybenzoylhydrazone) (107811-53-0) → {(OCH3C6H4CONNC(CH3))2UO2}

Guidance literature:

In ethanol; refluxing 6 h; elem. anal.;;

Reference yield: 90.0%

uranyl nirate hexahydrate + 2,3-butanedione bis(4-methoxybenzoylhydrazone) (107811-53-0) → {(OCH3C6H4CONHNC(CH3)C(CH3)NNCOC6H4OCH3)UO2}(1+)*NO3(1-)={(OCH3C6H4CONHNC(CH3)C(CH3)NNCOC6H4OCH3)UO2}(NO3)

Guidance literature:

In tetrahydrofuran; ethanol; addn. of an soln. of UO2(NO3)2*6H2O (1 mmol) to an soln. of the ligand (1 mmol) with stirring at room temperature for 12 h; filtration; washing with ethanol; drying in vac.; elem. anal.;

upstream raw materials:

4-methoxybenzoic acid hydrazide

dimethylglyoxal

Downstream raw materials:

1-<α-(p-Methoxy-benzoyloxy)-p-methoxy-benzylidenamino>-4,5-dimethyl-1,2,3-triazol