Technology Process of Sulfamide, [(3-nitrophenyl)methylene](1-phenylethyl)(phenylmethyl)-, (S)-
There total 5 articles about Sulfamide, [(3-nitrophenyl)methylene](1-phenylethyl)(phenylmethyl)-, (S)- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
Amberlyst 15; 5A molecular sieve;
In
benzene;
for 18h;
Heating;
DOI:10.1021/ja00245a030
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 83 percent / benzene / Heating
2: 90 percent / sodium borohydride
3: 78 percent / NH2SO2NH2 / 1,2-dimethoxy-ethane / 144 h / Heating
4: 77 percent / 5 A molecular sieves, Amberlyst 15 / benzene / 18 h / Heating
With
sodium tetrahydroborate; Amberlyst 15; 5A molecular sieve; SULFAMIDE;
In
1,2-dimethoxyethane; benzene;
DOI:10.1021/ja00245a030
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 78 percent / NH2SO2NH2 / 1,2-dimethoxy-ethane / 144 h / Heating
2: 77 percent / 5 A molecular sieves, Amberlyst 15 / benzene / 18 h / Heating
With
Amberlyst 15; 5A molecular sieve; SULFAMIDE;
In
1,2-dimethoxyethane; benzene;
DOI:10.1021/ja00245a030
