3H-3,8a-Etheno-1,2-benzodioxin-7-ol, 4,4a,5,6,7,8-hexahydro-4a,8,8-trimethyl-, benzoate

Base Information

Chemical Name:3H-3,8a-Etheno-1,2-benzodioxin-7-ol, 4,4a,5,6,7,8-hexahydro-4a,8,8-trimethyl-, benzoate
CAS No.:108511-78-0
Molecular Formula:C20H24O4
Molecular Weight:328.408
Hs Code.:
Mol file:108511-78-0.mol

Synonyms:

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Chemical Property of 3H-3,8a-Etheno-1,2-benzodioxin-7-ol, 4,4a,5,6,7,8-hexahydro-4a,8,8-trimethyl-, benzoate

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Technology Process of 3H-3,8a-Etheno-1,2-benzodioxin-7-ol, 4,4a,5,6,7,8-hexahydro-4a,8,8-trimethyl-, benzoate

There total 6 articles about 3H-3,8a-Etheno-1,2-benzodioxin-7-ol, 4,4a,5,6,7,8-hexahydro-4a,8,8-trimethyl-, benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 94759-83-8
2-(benzyloxy)-1,1,10-trimethyl-6,8-hexalin

: 108511-78-0
2-(benzyloxy)-1,1,10-trimethyl-6,9-epidioxy-Δ⁷-octalin

Guidance literature:: With polymer-bound Rose Bengal; oxygen; In dichloromethane; for 2.5h; Ambient temperature; Irradiation;
DOI:10.1021/jm00391a039

Reference yield:

: 4668-61-5
1,1,4a-trimethyl-3,4,4a,5,6,7-hexahydronaphthalen-2(1H)-one

: 108511-78-0
2-(benzyloxy)-1,1,10-trimethyl-6,9-epidioxy-Δ⁷-octalin

Guidance literature:: Multi-step reaction with 5 steps

1: 9.8 g / NaBH₄ / methanol / 0.67 h

2: 69 percent / pyridine / CHCl₃ / 3 h / Heating

3: N-bromosuccinimide (NBS), benzoyl peroxide / CCl₄ / 0.25 h / Heating

4: N,N-dimethylaniline / 0.5 h / Heating

5: 63 percent / oxygen, polymer-bound rose bengal / CH₂Cl₂ / 2.5 h / Ambient temperature; Irradiation

With pyridine; sodium tetrahydroborate; N-Bromosuccinimide; Perbenzoic acid; polymer-bound Rose Bengal; oxygen; N,N-dimethyl-aniline; In methanol; tetrachloromethane; dichloromethane; chloroform;
DOI:10.1021/jm00391a039

Reference yield:

: 91975-35-8
4,4,9-Trimethyl-Δ⁵⁽¹⁰⁾-octalol-(3)

: 108511-78-0
2-(benzyloxy)-1,1,10-trimethyl-6,9-epidioxy-Δ⁷-octalin

Guidance literature:: Multi-step reaction with 4 steps

1: 69 percent / pyridine / CHCl₃ / 3 h / Heating

2: N-bromosuccinimide (NBS), benzoyl peroxide / CCl₄ / 0.25 h / Heating

3: N,N-dimethylaniline / 0.5 h / Heating

4: 63 percent / oxygen, polymer-bound rose bengal / CH₂Cl₂ / 2.5 h / Ambient temperature; Irradiation

With pyridine; N-Bromosuccinimide; Perbenzoic acid; polymer-bound Rose Bengal; oxygen; N,N-dimethyl-aniline; In tetrachloromethane; dichloromethane; chloroform;
DOI:10.1021/jm00391a039