10b,10c-Dipropyl-10b,10c-dihydropyrene

Base Information

Chemical Name:10b,10c-Dipropyl-10b,10c-dihydropyrene
CAS No.:28816-94-6
Molecular Formula:C₂₂H₂₄
Molecular Weight:288.433
Hs Code.:
DSSTox Substance ID:DTXSID20951464
Nikkaji Number:J505.218A
Wikidata:Q82929783
Mol file:28816-94-6.mol

Synonyms:Pyrene, 10b,10c-dihydro-10b,10c-dipropyl-, trans-;28816-94-6;10b,10c-Dipropyl-10b,10c-dihydropyrene;DTXSID20951464;CNURFFWIKKDBJB-HZCBDIJESA-N;10b,10c-Dipropyl-10b,10c-dihydropyrene #;trans-10b,10c-Dihydro-10b,10c-dipropylpyrene

Suppliers and Price of 10b,10c-Dipropyl-10b,10c-dihydropyrene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of 10b,10c-Dipropyl-10b,10c-dihydropyrene

Chemical Property:

Vapor Pressure:8.18E-10mmHg at 25°C
Boiling Point:504.7°C at 760 mmHg
Flash Point:232.2°C
Density:1.07g/cm³
XLogP3:7.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:4
Exact Mass:288.187800766
Heavy Atom Count:22
Complexity:607

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCCC12C3=CC=C4C1(C(=CC=C4)C=CC2=CC=C3)CCC

Technology Process of 10b,10c-Dipropyl-10b,10c-dihydropyrene

There total 10 articles about 10b,10c-Dipropyl-10b,10c-dihydropyrene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 104-45-0
4-n-propylanisole

: 28816-94-6
trans-15,16-Di-n-propyldihydropyren

Guidance literature:: Multi-step reaction with 10 steps

2: 1-methyl-pyrrolidin-2-one / 170 - 180 °C

3: aq. KOH / Heating

4: H₂SO₄

5: LiAlH₄

6: PBr₃

7: Na

8: CrO₃, aq. H₂SO₄

9: O₂, KOH, MeOH

10: (i) LiAlH₄, AlCl₃, (ii) DDQ

With 1-methyl-pyrrolidin-2-one; chromium(VI) oxide; methanol; potassium hydroxide; lithium aluminium tetrahydride; sulfuric acid; oxygen; sodium; phosphorus tribromide;
DOI:10.1021/ja00715a021

Reference yield:

: 28746-13-6
3,5-Dibrom-4-n-propylanisol

: 28816-94-6
trans-15,16-Di-n-propyldihydropyren

Guidance literature:: Multi-step reaction with 9 steps

1: 1-methyl-pyrrolidin-2-one / 170 - 180 °C

2: aq. KOH / Heating

3: H₂SO₄

4: LiAlH₄

5: PBr₃

6: Na

7: CrO₃, aq. H₂SO₄

8: O₂, KOH, MeOH

9: (i) LiAlH₄, AlCl₃, (ii) DDQ

With 1-methyl-pyrrolidin-2-one; chromium(VI) oxide; methanol; potassium hydroxide; lithium aluminium tetrahydride; sulfuric acid; oxygen; sodium; phosphorus tribromide;
DOI:10.1021/ja00715a021

Reference yield:

: 28746-17-0
3,5-Bis(hydroxymethyl)-4-n-propylanisol

: 28816-94-6
trans-15,16-Di-n-propyldihydropyren

Guidance literature:: Multi-step reaction with 5 steps

1: PBr₃

2: Na

3: CrO₃, aq. H₂SO₄

4: O₂, KOH, MeOH

5: (i) LiAlH₄, AlCl₃, (ii) DDQ

With chromium(VI) oxide; methanol; potassium hydroxide; sulfuric acid; oxygen; sodium; phosphorus tribromide;
DOI:10.1021/ja00715a021