2-(4,7-Dimethylnaphthalene-1-carbonyl)benzoic acid

Base Information

Chemical Name:2-(4,7-Dimethylnaphthalene-1-carbonyl)benzoic acid
CAS No.:108712-23-8
Molecular Formula:C20H16O3
Molecular Weight:
Hs Code.:
DSSTox Substance ID:DTXSID30550063
Wikidata:Q82429275
Mol file:108712-23-8.mol

Synonyms:108712-23-8;2-(4,7-Dimethylnaphthalene-1-carbonyl)benzoic acid;2-(4,7-Dimethyl-1-naphthoyl)benzoic acid;DTXSID30550063

Suppliers and Price of 2-(4,7-Dimethylnaphthalene-1-carbonyl)benzoic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of 2-(4,7-Dimethylnaphthalene-1-carbonyl)benzoic acid

Chemical Property:

XLogP3:4.8
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:304.109944368
Heavy Atom Count:23
Complexity:458

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC2=C(C=CC(=C2C=C1)C)C(=O)C3=CC=CC=C3C(=O)O

Technology Process of 2-(4,7-Dimethylnaphthalene-1-carbonyl)benzoic acid

There total 1 articles about 2-(4,7-Dimethylnaphthalene-1-carbonyl)benzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 85-44-9
phthalic anhydride

: 575-43-9
1,6-dimethylnaphthalene

: 108712-23-8
2-(4,7-dimethylnaphthoyl)benzoic acid

Guidance literature:: DOI:10.1021/ja01335a050

Reference yield:

: 108712-23-8
2-(4,7-dimethylnaphthoyl)benzoic acid

: (R)-2-[(R)-3-(4,7-Dimethyl-naphthalen-1-yl)-3-methyl-3H-isobenzofuran-(1Z)-ylideneamino]-2-phenyl-ethanol

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / tetrahydrofuran / 1 h / -78 - 25 °C

2: 92 percent / Lawesson's reagent / toluene / 12 h / Heating

3: mercuric trifluoroacetate / tetrahydrofuran / 0.5 h / Ambient temperature

With Lawessons reagent; mercury(II) trifluoroacetate; In tetrahydrofuran; toluene;
DOI:10.1021/jo00390a012

Reference yield:

: 108712-23-8
2-(4,7-dimethylnaphthoyl)benzoic acid

: (R)-2-[(S)-3-(4,7-Dimethyl-naphthalen-1-yl)-3-methyl-3H-isobenzofuran-(1Z)-ylideneamino]-2-phenyl-ethanol

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / tetrahydrofuran / 1 h / -78 - 25 °C

2: 92 percent / Lawesson's reagent / toluene / 12 h / Heating

3: mercuric trifluoroacetate / tetrahydrofuran / 0.5 h / Ambient temperature

With Lawessons reagent; mercury(II) trifluoroacetate; In tetrahydrofuran; toluene;
DOI:10.1021/jo00390a012