3,8-dimethyl-2-(methylsulfanyl)-3H-imidazo[4,5-f]quinoxaline

Base Information

Chemical Name:3,8-dimethyl-2-(methylsulfanyl)-3H-imidazo[4,5-f]quinoxaline
CAS No.:108905-67-5
Molecular Formula:C12H12N4S
Molecular Weight:244.32
Hs Code.:
Mol file:108905-67-5.mol

Synonyms:3H-Imidazo[4,5-f]quinoxaline,3,8-dimethyl-2-(methylthio);3,8-dimethyl-2-(methylthio)-imidazo<4,5-f>quinoxaline;3,8-Dimethyl-2-methylsulfanylimidazo(4,5-f)quinoxaline;3,8-dimethyl-2-(methylsulfanyl)-3h-imidazo[4,5-f]quinoxaline;

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Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3,8-dimethyl-2-(methylsulfanyl)-3H-imidazo[4,5-f]quinoxaline

Chemical Property:

Vapor Pressure:3.24E-08mmHg at 25°C
Boiling Point:447.9oC at 760 mmHg
PKA:-0.46±0.50(Predicted)
Flash Point:224.7oC
PSA：68.90000
Density:1.37g/cm3
LogP:2.54680

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 3,8-dimethyl-2-(methylsulfanyl)-3H-imidazo[4,5-f]quinoxaline

There total 1 articles about 3,8-dimethyl-2-(methylsulfanyl)-3H-imidazo[4,5-f]quinoxaline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 108905-66-4
2-(5-methyl-2-pyrazinyl)-1-(4-bromo-1-methyl-2-(methylthio)-5-imidazolyl)ethene

: 108905-67-5
3,8-dimethyl-2-(methylthio)-imidazo<4,5-f>quinoxaline

Guidance literature:: With potassium tert-butylate; In tert-butyl alcohol; benzene; for 0.166667h; Irradiation;
DOI:10.1021/jo00031a017

Reference yield:

: 108905-67-5
3,8-dimethyl-2-(methylthio)-imidazo<4,5-f>quinoxaline

: 77500-04-0
2-amine-3,8-dimethylimidazo[4,5-f]quinoxaline

Guidance literature:: Multi-step reaction with 3 steps

1: 51.1 percent / aq. KMnO₄, glacial acetic acid / 0.75 h / Ambient temperature

2: 88 percent / 45 h / 140 - 150 °C

3: 72 percent / ammonium formate / 10percent Pd/C / methanol / 96 h / Heating

With potassium permanganate; ammonium formate; acetic acid; palladium on activated charcoal; In methanol;
DOI:10.1021/jo00031a017

Reference yield:

: 108905-67-5
3,8-dimethyl-2-(methylthio)-imidazo<4,5-f>quinoxaline

: 138336-27-3
2-(N-benzylamino)-3,8-dimethylimidazo<4,5-f>quinoxaline

Guidance literature:: Multi-step reaction with 2 steps

1: 51.1 percent / aq. KMnO₄, glacial acetic acid / 0.75 h / Ambient temperature

2: 88 percent / 45 h / 140 - 150 °C

With potassium permanganate; acetic acid;
DOI:10.1021/jo00031a017