Benzenethiol, 2,2'-[1,2-ethanediylbis(methylimino)]bis-

Base Information

Chemical Name:Benzenethiol, 2,2'-[1,2-ethanediylbis(methylimino)]bis-
CAS No.:109334-45-4
Molecular Formula:C16H20N2S2
Molecular Weight:304.48
Hs Code.:
DSSTox Substance ID:DTXSID20456742
Nikkaji Number:J814.298J
Wikidata:Q82279305
Mol file:109334-45-4.mol

Synonyms:Benzenethiol, 2,2'-[1,2-ethanediylbis(methylimino)]bis-;109334-45-4;DTXSID20456742;2,2'-[Ethylenebis(methylimino)]dibenzenethiol;n,n'-dimethyl-n,n'-bis(2-mercaptophenyl)ethylenediamine

Suppliers and Price of Benzenethiol, 2,2'-[1,2-ethanediylbis(methylimino)]bis-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzenethiol, 2,2'-[1,2-ethanediylbis(methylimino)]bis-

Chemical Property:

XLogP3:4.2
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:5
Exact Mass:304.10679099
Heavy Atom Count:20
Complexity:260

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CN(CCN(C)C1=CC=CC=C1S)C2=CC=CC=C2S

Technology Process of Benzenethiol, 2,2'-[1,2-ethanediylbis(methylimino)]bis-

There total 3 articles about Benzenethiol, 2,2'-[1,2-ethanediylbis(methylimino)]bis- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 109334-47-6
N,N'-dimethyl-N,N'-bis(2-S-benzylthiophenyl)ethylenediamine

: 109334-45-4
N,N'-dimethyl-N,N'-bis(2-S-mercaptophenyl)ethylenediamine

Guidance literature:: With sodium; In tetrahydrofuran; for 48h;

Reference yield:

: 109334-46-5
N-methyl-2-S-benzylthioaniline

: 109334-45-4
N,N'-dimethyl-N,N'-bis(2-S-mercaptophenyl)ethylenediamine

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) ZnCl₂, NaBH₃CN 2.) Na, n-butylalcohol / 1.) MeOH, RT, 3 h 2.) reflux

2: 65 percent / Na / butan-1-ol / 4 h / Heating

With sodium; sodium cyanoborohydride; zinc(II) chloride; butan-1-ol; In butan-1-ol;
DOI:10.1021/ja00253a016

Reference yield:

: 21749-63-3
2-(methylamino)benzenethiol

: 109334-45-4
N,N'-dimethyl-N,N'-bis(2-S-mercaptophenyl)ethylenediamine

Guidance literature:: Multi-step reaction with 3 steps

1: 98 percent / 2 N NaOH / ethanol; H₂O / 8 h / Ambient temperature

2: 1.) ZnCl₂, NaBH₃CN 2.) Na, n-butylalcohol / 1.) MeOH, RT, 3 h 2.) reflux

3: 65 percent / Na / butan-1-ol / 4 h / Heating

With sodium hydroxide; sodium; sodium cyanoborohydride; zinc(II) chloride; butan-1-ol; In ethanol; water; butan-1-ol;
DOI:10.1021/ja00253a016