Technology Process of Benzenepropanol, a-methyl-, acetate, (S)-
There total 24 articles about Benzenepropanol, a-methyl-, acetate, (S)- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
dicarbonyl(chloro)(η5-pentaphenylcyclopentadienyl)ruthenium(II); potassium tert-butylate; C. antarctica B immobilized lipase; sodium carbonate;
In
tetrahydrofuran; toluene;
at 60 ℃;
for 3h;
stereoselective reaction;
Schlenk technique;
Inert atmosphere;
Enzymatic reaction;
DOI:10.1021/acs.joc.1c00154
- Guidance literature:
-
With
dicarbonylchlorido(pentabenzylcyclopentadienyl)ruthenium; potassium tert-butylate; sodium carbonate;
In
tetrahydrofuran; toluene;
at 23 ℃;
for 3h;
optical yield given as %ee;
enantioselective reaction;
Inert atmosphere;
dynamic kinetic resolution;
Enzymatic reaction;
DOI:10.1002/ejoc.201001703
- Guidance literature:
-
4-Phenyl-2-butanone;
With
C51H41P2Ru(1+)*C32H12BF24(1-); potassium carbonate;
In
isopropyl alcohol; toluene;
at 70 ℃;
for 1h;
Glovebox;
Isopropenyl acetate;
With
Candida antarctica lipase B; C51H41P2Ru(1+)*C32H12BF24(1-);
In
toluene;
at 20 ℃;
for 16h;
enantioselective reaction;
DOI:10.1002/chem.201404096