1,3-Diazabicyclo[4.2.0]octane-2-carboxylic acid, 8-oxo-3-[(trifluoromethyl)sulfonyl]-, (4-nitrophenyl)methyl ester, cis-

Base Information

Chemical Name:1,3-Diazabicyclo[4.2.0]octane-2-carboxylic acid, 8-oxo-3-[(trifluoromethyl)sulfonyl]-, (4-nitrophenyl)methyl ester, cis-
CAS No.:109533-24-6
Molecular Formula:C₁₅H₁₄F₃N₃O₇S
Molecular Weight:437.353
Hs Code.:
Mol file:109533-24-6.mol

Synonyms:

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Chemical Property of 1,3-Diazabicyclo[4.2.0]octane-2-carboxylic acid, 8-oxo-3-[(trifluoromethyl)sulfonyl]-, (4-nitrophenyl)methyl ester, cis-

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Technology Process of 1,3-Diazabicyclo[4.2.0]octane-2-carboxylic acid, 8-oxo-3-[(trifluoromethyl)sulfonyl]-, (4-nitrophenyl)methyl ester, cis-

There total 4 articles about 1,3-Diazabicyclo[4.2.0]octane-2-carboxylic acid, 8-oxo-3-[(trifluoromethyl)sulfonyl]-, (4-nitrophenyl)methyl ester, cis- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 109533-20-2
4-(2-Bromethyl)-2-azetidinon

: 109533-24-6,109533-25-7
8-Oxo-3-(trifluormethylsulfonyl)-1,3-diazabicyclo<4.2.0>octan-2-carbonsaeure-p-nitrobenzylester

Guidance literature:: Multi-step reaction with 4 steps

1: 90 percent / Triton-A-azide / dimethylformamide / 48 h / Ambient temperature

2: 98 percent / H₂ / 10 percent Pd/C / methanol / 8 h / Ambient temperature

3: 51 percent / 6 h / Ambient temperature

4: N-Methylmorpholine / CH₂Cl₂ / 0.25 h / 0 °C

With 4-methyl-morpholine; Triton-A-azide; hydrogen; palladium on activated charcoal; In methanol; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 109533-21-3
4-(2-Azidoethyl)-2-azetidinon

: 109533-24-6,109533-25-7
8-Oxo-3-(trifluormethylsulfonyl)-1,3-diazabicyclo<4.2.0>octan-2-carbonsaeure-p-nitrobenzylester

Guidance literature:: Multi-step reaction with 3 steps

1: 98 percent / H₂ / 10 percent Pd/C / methanol / 8 h / Ambient temperature

2: 51 percent / 6 h / Ambient temperature

3: N-Methylmorpholine / CH₂Cl₂ / 0.25 h / 0 °C

With 4-methyl-morpholine; hydrogen; palladium on activated charcoal; In methanol; dichloromethane;