(2-Butyl-3,3-dimethylcycloprop-1-en-1-yl)benzene

Base Information

Chemical Name:(2-Butyl-3,3-dimethylcycloprop-1-en-1-yl)benzene
CAS No.:109900-82-5
Molecular Formula:C15H20
Molecular Weight:200.324
Hs Code.:
DSSTox Substance ID:DTXSID60547300
Wikidata:Q82425431
Mol file:109900-82-5.mol

Synonyms:109900-82-5;(2-Butyl-3,3-dimethylcycloprop-1-en-1-yl)benzene;DTXSID60547300

Suppliers and Price of (2-Butyl-3,3-dimethylcycloprop-1-en-1-yl)benzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2-Butyl-3,3-dimethylcycloprop-1-en-1-yl)benzene

Chemical Property:

XLogP3:4.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:4
Exact Mass:200.156500638
Heavy Atom Count:15
Complexity:251

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCCCC1=C(C1(C)C)C2=CC=CC=C2

Technology Process of (2-Butyl-3,3-dimethylcycloprop-1-en-1-yl)benzene

There total 7 articles about (2-Butyl-3,3-dimethylcycloprop-1-en-1-yl)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 109-72-8,29786-93-4
n-butyllithium

: 109900-82-5
1-(3,3-dimethyl-2-phenylcyclopropen-1-yl)-1-butane

Guidance literature:: With ammonium chloride; In tetrahydrofuran; hexane; 1.) -78 deg C, 1 h, 2.) 0 deg C, 3 h;
DOI:10.1016/S0040-4039(00)85335-6

Reference yield: 81.0%

: 109-72-8,29786-93-4
n-butyllithium

: 119145-30-1
3,3-dimethyl-1-(methylsulfonyl)-2-phenylcyclopropene

: 109900-82-5
1-(3,3-dimethyl-2-phenylcyclopropen-1-yl)-1-butane

Guidance literature:: In tetrahydrofuran; 1.) -78 deg C, 1 h, 2.) 0 deg C, 30 min;
DOI:10.1021/jo00268a026

Reference yield:

: 5324-64-1
2-(benzenesulfonyl)ethynylbenzene

: 109900-82-5
1-(3,3-dimethyl-2-phenylcyclopropen-1-yl)-1-butane

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / diethyl ether / 1.) -78 deg C, 30 min, 2.) 25 deg C, 12 h

2: 95 percent / benzene / 1.5 h / Irradiation

3: 85 percent / tetrahydrofuran / 1.) -78 deg C, 1 h, 2.) 0 deg C, 30 min

In tetrahydrofuran; diethyl ether; benzene;
DOI:10.1021/jo00268a026