2-Phenyl-9H-carbazole-1-carbaldehyde

Base Information

Chemical Name:2-Phenyl-9H-carbazole-1-carbaldehyde
CAS No.:110110-38-8
Molecular Formula:C19H13NO
Molecular Weight:271.318
Hs Code.:
DSSTox Substance ID:DTXSID40551440
Nikkaji Number:J3.379.963B
Wikidata:Q82431104

Synonyms:2-PHENYL-9H-CARBAZOLE-1-CARBALDEHYDE;110110-38-8;SCHEMBL4582415;DTXSID40551440

Suppliers and Price of 2-Phenyl-9H-carbazole-1-carbaldehyde

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-Phenyl-9H-carbazole-1-carbaldehyde

Chemical Property:

XLogP3:4.5
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:2
Exact Mass:271.099714038
Heavy Atom Count:21
Complexity:376

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)C2=C(C3=C(C=C2)C4=CC=CC=C4N3)C=O

Technology Process of 2-Phenyl-9H-carbazole-1-carbaldehyde

There total 4 articles about 2-Phenyl-9H-carbazole-1-carbaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 21.0%

: 14371-10-9
(E)-3-phenylpropenal

: 3156-51-2,51870-94-1
3-[(E)-2-nitroeth-1-enyl]-1H-indole

: 110110-38-8
2-Phenyl-9H-carbazole-1-carbaldehyde

Guidance literature:: With hydroquinone; at 130 - 140 ℃; for 21h;

Reference yield:

: C₁₉H₁₅NO

: 110110-38-8
2-Phenyl-9H-carbazole-1-carbaldehyde

Guidance literature:: With manganese(IV) oxide; In dichloromethane; at 20 ℃; for 14h; Inert atmosphere;
DOI:10.1055/s-0034-1378446

Reference yield:

: 14371-10-9
(E)-3-phenylpropenal

: 110110-38-8
2-Phenyl-9H-carbazole-1-carbaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1.1: 1,4-diaza-bicyclo[2.2.2]octane / water / 60 °C / Green chemistry

1.2: air / 48 h / 60 °C / Green chemistry

2.1: diisobutylaluminium hydride / toluene / 2 h / 0 °C

3.1: manganese(IV) oxide / dichloromethane / 14 h / 20 °C / Inert atmosphere

With 1,4-diaza-bicyclo[2.2.2]octane; manganese(IV) oxide; diisobutylaluminium hydride; In dichloromethane; water; toluene;
DOI:10.1055/s-0034-1378446