Benzoic acid, 4-chloro-2-((3-methylphenyl)amino)-, ((4,5-dimethoxy-2-nitrophenyl)methylene)hydrazide

Base Information

Chemical Name:Benzoic acid, 4-chloro-2-((3-methylphenyl)amino)-, ((4,5-dimethoxy-2-nitrophenyl)methylene)hydrazide
CAS No.:75423-00-6
Molecular Formula:C₂₃H₂₁ClN₄O₅
Molecular Weight:468.897
Hs Code.:

Synonyms:BRN 4603755;Benzoic acid, 4-chloro-2-((3-methylphenyl)amino)-, ((4,5-dimethoxy-2-nitrophenyl)methylene)hydrazide;75423-00-6;LS-36545

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzoic acid, 4-chloro-2-((3-methylphenyl)amino)-, ((4,5-dimethoxy-2-nitrophenyl)methylene)hydrazide

Chemical Property:

XLogP3:5.7
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:7
Rotatable Bond Count:7
Exact Mass:468.1200475
Heavy Atom Count:33
Complexity:690

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC(=CC=C1)NC2=C(C=CC(=C2)Cl)C(=O)NN=CC3=CC(=C(C=C3[N+](=O)[O-])OC)OC
Isomeric SMILES:CC1=CC(=CC=C1)NC2=C(C=CC(=C2)Cl)C(=O)N/N=C/C3=CC(=C(C=C3[N+](=O)[O-])OC)OC

Technology Process of Benzoic acid, 4-chloro-2-((3-methylphenyl)amino)-, ((4,5-dimethoxy-2-nitrophenyl)methylene)hydrazide

There total 5 articles about Benzoic acid, 4-chloro-2-((3-methylphenyl)amino)-, ((4,5-dimethoxy-2-nitrophenyl)methylene)hydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 50-84-0
2,4 dichlorobenzoic acid

: 75423-00-6
4-Chloro-2-m-tolylamino-benzoic acid [1-(4,5-dimethoxy-2-nitro-phenyl)-meth-(E)-ylidene]-hydrazide

Guidance literature:: Multi-step reaction with 4 steps

1: K₂CO₃, copper powder / pentan-1-ol

2: SOCl₂ / 12 h / Heating

3: hydrazine hydrate / ethanol / 16 h / Heating

4: gl. acetic acid / ethanol / 4 h / Heating

With thionyl chloride; copper; potassium carbonate; hydrazine hydrate; acetic acid; In ethanol; pentan-1-ol;

Reference yield:

: 32305-29-6
4-chloro-2-m-toluidino-benzoic acid

: 75423-00-6
4-Chloro-2-m-tolylamino-benzoic acid [1-(4,5-dimethoxy-2-nitro-phenyl)-meth-(E)-ylidene]-hydrazide

Guidance literature:: Multi-step reaction with 3 steps

1: SOCl₂ / 12 h / Heating

2: hydrazine hydrate / ethanol / 16 h / Heating

3: gl. acetic acid / ethanol / 4 h / Heating

With thionyl chloride; hydrazine hydrate; acetic acid; In ethanol;

Reference yield:

: 77817-52-8
4-Chloro-2-m-tolylamino-benzoic acid methyl ester

: 75423-00-6
4-Chloro-2-m-tolylamino-benzoic acid [1-(4,5-dimethoxy-2-nitro-phenyl)-meth-(E)-ylidene]-hydrazide

Guidance literature:: Multi-step reaction with 2 steps

1: hydrazine hydrate / ethanol / 16 h / Heating

2: gl. acetic acid / ethanol / 4 h / Heating

With hydrazine hydrate; acetic acid; In ethanol;