Benzaldehyde, 3-[[[(1,1-dimethylethyl)diphenylsilyl]oxy]methyl]-

Base Information

Chemical Name:Benzaldehyde, 3-[[[(1,1-dimethylethyl)diphenylsilyl]oxy]methyl]-
CAS No.:110130-71-7
Molecular Formula:C24H26O2Si
Molecular Weight:374.555
Hs Code.:
DSSTox Substance ID:DTXSID10447028
Mol file:110130-71-7.mol

Synonyms:110130-71-7;Benzaldehyde, 3-[[[(1,1-dimethylethyl)diphenylsilyl]oxy]methyl]-;SCHEMBL8018718;DTXSID10447028;MUHKOIACOCBEND-UHFFFAOYSA-N;3-t-butyldiphenylsilyloxymethylbenzaldehyde;3-(((tert-butyldiphenylsilyl)oxy)methyl)benzaldehyde

Suppliers and Price of Benzaldehyde, 3-[[[(1,1-dimethylethyl)diphenylsilyl]oxy]methyl]-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzaldehyde, 3-[[[(1,1-dimethylethyl)diphenylsilyl]oxy]methyl]-

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:7
Exact Mass:374.170206602
Heavy Atom Count:27
Complexity:440

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C)(C)[Si](C1=CC=CC=C1)(C2=CC=CC=C2)OCC3=CC(=CC=C3)C=O

Technology Process of Benzaldehyde, 3-[[[(1,1-dimethylethyl)diphenylsilyl]oxy]methyl]-

There total 5 articles about Benzaldehyde, 3-[[[(1,1-dimethylethyl)diphenylsilyl]oxy]methyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 144543-20-4
[3-({[tert-butyl(diphenyl)silyl]oxy}methyl)phenyl]methanol

: 110130-71-7
3-(((tert-butyldiphenylsilyl)oxy)methyl)benzaldehyde

Guidance literature:: With Dess-Martin periodane; In dichloromethane; at 20 ℃;
DOI:10.1016/j.bmcl.2010.10.140

Reference yield:

: 626-19-7
Isophthalaldehyde

: 110130-71-7
3-(((tert-butyldiphenylsilyl)oxy)methyl)benzaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: 3 g / NaBH₄ / ethanol / Ambient temperature

2: 8.98 g / triethylamine, 4-pyrrolidinopyridine / CH₂Cl₂ / Ambient temperature

With sodium tetrahydroborate; 4-pyrrolidin-1-ylpyridine; triethylamine; In ethanol; dichloromethane;