14-Methyl-5α-cholest-8-ene-3β,6α-diol

Base Information

• Chemical Name: 14-Methyl-5α-cholest-8-ene-3β,6α-diol
• CAS No.: 2126-69-4
• Molecular Formula: C₂₈H₄₈O₂
• Molecular Weight: 416.688
• Mol file: 2126-69-4.mol

Synonyms:(3S,5S,6S,10S,13R,14R,17R)-17-((R)-1,5-Dimethyl-hexyl)-10,13,14-trimethyl-2,3,4,5,6,7,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthrene-3,6-diol;

Chemical Property of 14-Methyl-5α-cholest-8-ene-3β,6α-diol

Chemical Property:

• Melting Point: 173-174.5 °C
• Boiling Point: 515.9±50.0 °C(Predicted)
• PKA: 14.69±0.70(Predicted)
• PSA: 40.46000
• Density: 1.03±0.1 g/cm3(Predicted)
• LogP: 6.89370

Purity/Quality:

98.5% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 14-Methyl-5α-cholest-8-ene-3β,6α-diol

There total 1 articles about 14-Methyl-5α-cholest-8-ene-3β,6α-diol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ Macdougallin (14α-Methyl-Δ8-cholesten-3β,6α-diol) (2126-69-4)

Guidance literature:

Diacetat (Abtrennung von Peniocerol-diacetat durch frakt. Kristallisation), alkal. Verseifung;

DOI:10.1021/ja00889a056

Reference yield:

macdougallin (2126-69-4) + p-toluenesulfonyl chloride (98-59-9) → macdougallin ditosylate

Guidance literature:

In chloroform; at 20 ℃;

DOI:10.1016/j.phytochem.2005.07.010