Benzenemethanamine, N,N-bis(2,2-diethoxyethyl)-

Base Information

Chemical Name:Benzenemethanamine, N,N-bis(2,2-diethoxyethyl)-
CAS No.:110376-66-4
Molecular Formula:C19H33NO4
Molecular Weight:339.47000
Hs Code.:
NSC Number:174611
DSSTox Substance ID:DTXSID10306202
Wikidata:Q82053175
Mol file:110376-66-4.mol

Synonyms:Benzenemethanamine, N,N-bis(2,2-diethoxyethyl)-;110376-66-4;NSC174611;DTXSID10306202;ADAL1038984;AKOS024329352;NSC-174611;BENZYLBIS(2,2-DIETHOXYETHYL)AMINE;N-benzyl-N,N-bis(2,2-diethoxyethyl)amine

Suppliers and Price of Benzenemethanamine, N,N-bis(2,2-diethoxyethyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Benzenemethanamine, N,N-bis(2,2-diethoxyethyl)-

Chemical Property:

PSA：40.16000
LogP:3.28680
XLogP3:3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:14
Exact Mass:339.24095853
Heavy Atom Count:24
Complexity:255

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCOC(CN(CC1=CC=CC=C1)CC(OCC)OCC)OCC

Technology Process of Benzenemethanamine, N,N-bis(2,2-diethoxyethyl)-

There total 2 articles about Benzenemethanamine, N,N-bis(2,2-diethoxyethyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 37.0%

: 2032-35-1
Bromoacetaldehyde diethyl acetal

: 100-46-9
benzylamine

: 110376-66-4
benzyl-bis-(2,2-diethoxy-ethyl)-amine

Guidance literature:: With triethylamine; at 100 ℃; for 18h; Inert atmosphere;
DOI:10.1021/acs.orglett.9b00378

Reference yield:

: 67856-69-3
iminodiacetaldehyde bis(diethyl acetal)

: 100-44-7
benzyl chloride

: 110376-66-4
benzyl-bis-(2,2-diethoxy-ethyl)-amine

Guidance literature:

Reference yield:

: 110376-66-4
benzyl-bis-(2,2-diethoxy-ethyl)-amine

: C₂₁H₃₇N₃O₅

Guidance literature:: Multi-step reaction with 3 steps

1.1: hydrogen; palladium 10% on activated carbon / ethanol / 4 h / 20 °C

2.1: N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 0.5 h / Inert atmosphere

2.2: Inert atmosphere

3.1: hydrazine hydrate / ethanol; water; toluene / 2 h / Reflux

With palladium 10% on activated carbon; hydrogen; hydrazine hydrate; N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; In ethanol; water; N,N-dimethyl-formamide; toluene;