2,4-Dichloro-1,3,5-trinitrobenzene

Base Information

• Chemical Name: 2,4-Dichloro-1,3,5-trinitrobenzene
• CAS No.: 1630-09-7
• Molecular Formula: C6HCl2N3O6
• Molecular Weight: 281.996
• Hs Code.: 2904909090
• European Community (EC) Number: 290-551-5
• DSSTox Substance ID: DTXSID70391770
• Nikkaji Number: J80.267K
• Wikidata: Q82189470
• Mol file: 1630-09-7.mol

Synonyms:2,4-dichloro-1,3,5-trinitrobenzene;1630-09-7;1,3-DICHLORO-2,4,6-TRINITROBENZENE;Styphnyl chloride;2,4-dichloro-1,3,5-trinitro-benzene;SCHEMBL7644871;DTXSID70391770;EINECS 290-551-5;STL371282;AKOS003239245;90171-11-2;Benzene, 2,4-dichloro-1,3,5-trinitro-;FT-0633718;Benzene, 2,4-dichloro-1,3,5-trinitro-, copper-coupled

Chemical Property of 2,4-Dichloro-1,3,5-trinitrobenzene

Chemical Property:

• Vapor Pressure: 1.23E-05mmHg at 25°C
• Melting Point: 126.5-127 °C
• Refractive Index: 1.671
• Boiling Point: 380 °C at 760 mmHg
• Flash Point: 183.6 °C
• PSA: 137.46000
• Density: 1.894g/cm³
• LogP: 4.28760
• XLogP3: 3.4
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 6
• Rotatable Bond Count: 0
• Exact Mass: 280.9242401
• Heavy Atom Count: 17
• Complexity: 323

Purity/Quality:

99% ^*data from raw suppliers

2,4-DICHLORO-1,3,5-TRINITROBENZENE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=C(C(=C(C(=C1[N+](=O)[O-])Cl)[N+](=O)[O-])Cl)[N+](=O)[O-]

Technology Process of 2,4-Dichloro-1,3,5-trinitrobenzene

There total 17 articles about 2,4-Dichloro-1,3,5-trinitrobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

chloromethoxy-1,3,5-trinitrobenzene (2845-90-1) → 2,4-dichloro-1,3,5-trinitrobenzene (1630-09-7)

Guidance literature:

With trichlorophosphate; In N,N-dimethyl-formamide; toluene; Heating;

DOI:10.1016/0040-4020(96)00201-3

Reference yield: 76.0%

1-bromo-3-methoxy-2,4,6-trinitrobenzene (21212-69-1) → 2,4-dichloro-1,3,5-trinitrobenzene (1630-09-7)

Guidance literature:

With trichlorophosphate; In N,N-dimethyl-formamide; toluene; Heating;

DOI:10.1016/0040-4020(96)00201-3

Reference yield: 73.0%

3-chloro-2,4,6-trinitro-phenol; potassium-(3-chloro-2.4.6-trinitro-phenolate) (60764-03-6) → 2,4-dichloro-1,3,5-trinitrobenzene (1630-09-7)

Guidance literature:

With trichlorophosphate; at 100 - 120 ℃; for 0.75h;

DOI:10.1016/0040-4020(96)00201-3

upstream raw materials:

2,4-dichloro-1,5-dinitrobenzene

1-chloro-2,4-dinitrochlorobenzene

3-chloro-2,4,6-trinitro-phenol

p-toluenesulfonyl chloride

Downstream raw materials:

2,4-Difluor-1,3,5-trinitro-benzol

4,4'-(2,4,6-trinitro-1,3-phenylene)bis(oxy)bis(3-nitrofurazan)

piperonal-(3-chloro-2,4,6-trinitro-phenylhydrazone)

formaldehyde-(3-chloro-2,4,6-trinitro-phenylhydrazone)