9,10-Anthracenedione, 1-hydroxy-5,8-dimethoxy-2-[2-(2-methyl-1,3-dioxolan-2-yl)ethyl]-3-[2-[(4- methylphenyl)sulfonyl]-2-(methylthio)ethyl]-

Base Information

Chemical Name:9,10-Anthracenedione, 1-hydroxy-5,8-dimethoxy-2-[2-(2-methyl-1,3-dioxolan-2-yl)ethyl]-3-[2-[(4- methylphenyl)sulfonyl]-2-(methylthio)ethyl]-
CAS No.:110419-45-9
Molecular Formula:C32H34O9S2
Molecular Weight:626.749
Hs Code.:
Mol file:110419-45-9.mol

9,10-Anthracenedione,
1-hydroxy-5,8-dimethoxy-2-[2-(2-methyl-1,3-dioxolan-2-yl)ethyl]-3-[2-[(4-
methylphenyl)sulfonyl]-2-(methylthio)ethyl]-

Synonyms:

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Chemical Property of 9,10-Anthracenedione, 1-hydroxy-5,8-dimethoxy-2-[2-(2-methyl-1,3-dioxolan-2-yl)ethyl]-3-[2-[(4- methylphenyl)sulfonyl]-2-(methylthio)ethyl]-

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Technology Process of 9,10-Anthracenedione, 1-hydroxy-5,8-dimethoxy-2-[2-(2-methyl-1,3-dioxolan-2-yl)ethyl]-3-[2-[(4- methylphenyl)sulfonyl]-2-(methylthio)ethyl]-

There total 5 articles about 9,10-Anthracenedione, 1-hydroxy-5,8-dimethoxy-2-[2-(2-methyl-1,3-dioxolan-2-yl)ethyl]-3-[2-[(4- methylphenyl)sulfonyl]-2-(methylthio)ethyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 96303-31-0
2-chloromethyl-1-hydroxy-5,8-dimethoxy-3-methyl-9,10-anthraquinone

: 110419-45-9
1-Hydroxy-5,8-dimethoxy-2-<2-(2-methyl-1,3-dioxolan-2-yl)-ethyl>-3-<2-(4-methylphenylsulfonyl)-2-(methylthio)ethyl>-9,10-anthrachinon

Guidance literature:: Multi-step reaction with 5 steps

2: 86 percent / 4-(dimethylamino)pyridine / CH₂Cl₂ / 1 h

3: 58 percent / N-bromosuccinimide / CCl₄ / 0.67 h / Heating; Irradiation

4: 96 percent / p-CH₃C₆H₄SO₃H, CH(OCH₃)3 / toluene / 4 h / 50 °C

With dmap; N-Bromosuccinimide; toluene-4-sulfonic acid; trimethyl orthoformate; In tetrachloromethane; dichloromethane; toluene;

Reference yield:

: 110419-29-9
1-Hydroxy-5,8-dimethoxy-3-methyl-2-(3-oxobutyl)-9,10-anthrachinon

: 110419-45-9
1-Hydroxy-5,8-dimethoxy-2-<2-(2-methyl-1,3-dioxolan-2-yl)-ethyl>-3-<2-(4-methylphenylsulfonyl)-2-(methylthio)ethyl>-9,10-anthrachinon

Guidance literature:: Multi-step reaction with 4 steps

1: 86 percent / 4-(dimethylamino)pyridine / CH₂Cl₂ / 1 h

2: 58 percent / N-bromosuccinimide / CCl₄ / 0.67 h / Heating; Irradiation

3: 96 percent / p-CH₃C₆H₄SO₃H, CH(OCH₃)3 / toluene / 4 h / 50 °C

With dmap; N-Bromosuccinimide; toluene-4-sulfonic acid; trimethyl orthoformate; In tetrachloromethane; dichloromethane; toluene;

Reference yield:

: 110419-30-2
1-(2,2-Dimethylpropionyloxy)-5,8-dimethoxy-3-methyl-2-(3-oxobutyl)-9,10-anthrachinon

: 110419-45-9
1-Hydroxy-5,8-dimethoxy-2-<2-(2-methyl-1,3-dioxolan-2-yl)-ethyl>-3-<2-(4-methylphenylsulfonyl)-2-(methylthio)ethyl>-9,10-anthrachinon

Guidance literature:: Multi-step reaction with 3 steps

1: 58 percent / N-bromosuccinimide / CCl₄ / 0.67 h / Heating; Irradiation

2: 96 percent / p-CH₃C₆H₄SO₃H, CH(OCH₃)3 / toluene / 4 h / 50 °C

With N-Bromosuccinimide; toluene-4-sulfonic acid; trimethyl orthoformate; In tetrachloromethane; toluene;