3-Aminomethyl-5,6-dihydroxyphthalide hydrobromide

Base Information

Chemical Name:3-Aminomethyl-5,6-dihydroxyphthalide hydrobromide
CAS No.:78219-03-1
Molecular Formula:BrH*C₉H₉NO₄
Molecular Weight:276.087
Hs Code.:2932209090
DSSTox Substance ID:DTXSID30999493
Mol file:78219-03-1.mol

Synonyms:78219-03-1;3-Aminomethyl-5,6-dihydroxyphthalide hydrobromide;Phthalide, 3-aminomethyl-5,6-dihydroxy-, hydrobromide;P 5;C9H9NO4.BrH;DTXSID30999493;LS-109383;1(3H)-Isobenzofuranone, 3-(aminomethyl)-5,6-dihydroxy-, hydrobromide;3-(Aminomethyl)-5,6-dihydroxy-2-benzofuran-1(3H)-one--hydrogen bromide (1/1)

Suppliers and Price of 3-Aminomethyl-5,6-dihydroxyphthalide hydrobromide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
3-AMINOMETHYL-5,6-DIHYDROXYPHTHALIDE HYDROBROMIDE 95.00%
5MG
$ 497.26

Total 3 raw suppliers

Chemical Property of 3-Aminomethyl-5,6-dihydroxyphthalide hydrobromide

Chemical Property:

Vapor Pressure:2.6E-11mmHg at 25°C
Boiling Point:517.1°C at 760 mmHg
Flash Point:266.5°C
PSA：92.78000
LogP:1.92640
Hydrogen Bond Donor Count:4
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:1
Exact Mass:274.97932
Heavy Atom Count:15
Complexity:245

Purity/Quality:

99% ^*data from raw suppliers

3-AMINOMETHYL-5,6-DIHYDROXYPHTHALIDE HYDROBROMIDE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=C2C(OC(=O)C2=CC(=C1O)O)CN.Br

Technology Process of 3-Aminomethyl-5,6-dihydroxyphthalide hydrobromide

There total 4 articles about 3-Aminomethyl-5,6-dihydroxyphthalide hydrobromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

: 103797-23-5
1-(aminomethyl)-5,6-dimethoxyphthalide hydrochloride

: 78219-03-1
1-(aminomethyl)-5,6-dihydroxyphthalide hydrobromide

Guidance literature:: With hydrogen bromide; for 4.5h; Heating;
DOI:10.1021/jm00384a030

Reference yield:

: 577-68-4
m-hemipinic acid

: 78219-03-1
1-(aminomethyl)-5,6-dihydroxyphthalide hydrobromide

Guidance literature:: Multi-step reaction with 3 steps

1: aq. NaOH

2: H₂ / Pd/C

3: 41 percent / 48percent HBr / 4.5 h / Heating

With sodium hydroxide; hydrogen bromide; hydrogen; palladium on activated charcoal;
DOI:10.1021/jm00384a030

Reference yield:

: 103989-27-1
5,6-dimethoxy-3-nitromethyl-phthalide

: 78219-03-1
1-(aminomethyl)-5,6-dihydroxyphthalide hydrobromide

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / Pd/C

2: 41 percent / 48percent HBr / 4.5 h / Heating

With hydrogen bromide; hydrogen; palladium on activated charcoal;
DOI:10.1021/jm00384a030