Phenol, 2,4,6-trinitro-, ytterbium(3+) salt, octahydrate

Base Information

• Chemical Name: Phenol, 2,4,6-trinitro-, ytterbium(3+) salt, octahydrate
• CAS No.: 111053-17-9
• Molecular Formula: 3C₆H₂N₃O₇*8H₂O*Yb
• Molecular Weight: 1001.46
• Mol file: 111053-17-9.mol

Synonyms:

Chemical Property of Phenol, 2,4,6-trinitro-, ytterbium(3+) salt, octahydrate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Phenol, 2,4,6-trinitro-, ytterbium(3+) salt, octahydrate

There total 1 articles about Phenol, 2,4,6-trinitro-, ytterbium(3+) salt, octahydrate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

ytterbium(III) carbonate hydrate + 2,4,6-Trinitrophenol (88-89-1) → ytterbium(III) picrate octahydrate (105136-73-0,111053-17-9)

Guidance literature:

With water; In water; picric acid dissolved in hot water; Yb carbonate portionwise added with stirring on water bath at 80-90°C, stirring continued for addnl. 10 min at that temp., hot mixt. filtered, cooled with ice; ppt. recrystd. 3 times from water, air-dried at room temp. for more than one week; elem. anal.;

DOI:10.1246/bcsj.60.2037

upstream raw materials:

2,4,6-Trinitrophenol