Benzoic acid, 4-[2-[2-[(2,2-dimethyl-1-oxopropyl)amino]-1,4-dihydro-4-oxo-6-pteridinyl ]ethyl]-, 1,1-dimethylethyl ester

Base Information

Chemical Name:Benzoic acid, 4-[2-[2-[(2,2-dimethyl-1-oxopropyl)amino]-1,4-dihydro-4-oxo-6-pteridinyl ]ethyl]-, 1,1-dimethylethyl ester
CAS No.:111292-02-5
Molecular Formula:C24H29N5O4
Molecular Weight:451.525
Hs Code.:
Mol file:111292-02-5.mol

Synonyms:

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Chemical Property of Benzoic acid, 4-[2-[2-[(2,2-dimethyl-1-oxopropyl)amino]-1,4-dihydro-4-oxo-6-pteridinyl ]ethyl]-, 1,1-dimethylethyl ester

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Technology Process of Benzoic acid, 4-[2-[2-[(2,2-dimethyl-1-oxopropyl)amino]-1,4-dihydro-4-oxo-6-pteridinyl ]ethyl]-, 1,1-dimethylethyl ester

There total 7 articles about Benzoic acid, 4-[2-[2-[(2,2-dimethyl-1-oxopropyl)amino]-1,4-dihydro-4-oxo-6-pteridinyl ]ethyl]-, 1,1-dimethylethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 59247-47-1
tert-butyl-4-bromobenzoate

: 111292-02-5
tert-butyl 4-<<2-(pivaloylamino)-4(3H)-oxopteridin-6-yl>ethyl>benzoate

Guidance literature:: Multi-step reaction with 5 steps

1: triphenylphosphine, palladium acetate, triethylamine / 12 h / 100 °C

2: potassium carbonate / methanol / 3 h / Ambient temperature

3: 54 percent / palladium acetate, tri-o-tolylphosphine, copper(I) iodide, triethylamine / acetonitrile / 16 h / 100 °C

4: H₂ / 10percent Pd/C / CH₂Cl₂; methanol / 0.75 h / Ambient temperature

5: O₂ / methanol; CH₂Cl₂ / 72 h / Ambient temperature

With copper(l) iodide; hydrogen; oxygen; palladium diacetate; potassium carbonate; triethylamine; triphenylphosphine; tris-(o-tolyl)phosphine; palladium on activated charcoal; In methanol; dichloromethane; acetonitrile;
DOI:10.1021/jo00236a009

Reference yield:

: 111291-97-5
4-ethynylbenzoic acid tert-butyl ester

: 111292-02-5
tert-butyl 4-<<2-(pivaloylamino)-4(3H)-oxopteridin-6-yl>ethyl>benzoate

Guidance literature:: Multi-step reaction with 3 steps

1: 54 percent / palladium acetate, tri-o-tolylphosphine, copper(I) iodide, triethylamine / acetonitrile / 16 h / 100 °C

2: H₂ / 10percent Pd/C / CH₂Cl₂; methanol / 0.75 h / Ambient temperature

3: O₂ / methanol; CH₂Cl₂ / 72 h / Ambient temperature

With copper(l) iodide; hydrogen; oxygen; palladium diacetate; triethylamine; tris-(o-tolyl)phosphine; palladium on activated charcoal; In methanol; dichloromethane; acetonitrile;
DOI:10.1021/jo00236a009

Reference yield:

: 111291-96-4
tert-butyl 4-<(trimethylsilyl)ethynyl>benzoate

: 111292-02-5
tert-butyl 4-<<2-(pivaloylamino)-4(3H)-oxopteridin-6-yl>ethyl>benzoate

Guidance literature:: Multi-step reaction with 4 steps

1: potassium carbonate / methanol / 3 h / Ambient temperature

2: 54 percent / palladium acetate, tri-o-tolylphosphine, copper(I) iodide, triethylamine / acetonitrile / 16 h / 100 °C

3: H₂ / 10percent Pd/C / CH₂Cl₂; methanol / 0.75 h / Ambient temperature

4: O₂ / methanol; CH₂Cl₂ / 72 h / Ambient temperature

With copper(l) iodide; hydrogen; oxygen; palladium diacetate; potassium carbonate; triethylamine; tris-(o-tolyl)phosphine; palladium on activated charcoal; In methanol; dichloromethane; acetonitrile;
DOI:10.1021/jo00236a009