Uridine, 2'-O-[1,4-dimethoxy-1-(3-methoxy-3-oxopropyl)-4-oxobutyl]-4-O-(6-meth yl-3-pyridinyl)-5'-O-[9-[4-(octadecyloxy)phenyl]-9H-xanthen-9-yl]-

Base Information

Chemical Name:Uridine, 2'-O-[1,4-dimethoxy-1-(3-methoxy-3-oxopropyl)-4-oxobutyl]-4-O-(6-meth yl-3-pyridinyl)-5'-O-[9-[4-(octadecyloxy)phenyl]-9H-xanthen-9-yl]-
CAS No.:111447-40-6
Molecular Formula:C₆₂H₈₁N₃O₁₃
Molecular Weight:1076.34
Hs Code.:
Mol file:111447-40-6.mol

Synonyms:

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Chemical Property of Uridine, 2'-O-[1,4-dimethoxy-1-(3-methoxy-3-oxopropyl)-4-oxobutyl]-4-O-(6-meth yl-3-pyridinyl)-5'-O-[9-[4-(octadecyloxy)phenyl]-9H-xanthen-9-yl]-

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Technology Process of Uridine, 2'-O-[1,4-dimethoxy-1-(3-methoxy-3-oxopropyl)-4-oxobutyl]-4-O-(6-meth yl-3-pyridinyl)-5'-O-[9-[4-(octadecyloxy)phenyl]-9H-xanthen-9-yl]-

There total 6 articles about Uridine, 2'-O-[1,4-dimethoxy-1-(3-methoxy-3-oxopropyl)-4-oxobutyl]-4-O-(6-meth yl-3-pyridinyl)-5'-O-[9-[4-(octadecyloxy)phenyl]-9H-xanthen-9-yl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 95985-07-2
9-chloro-9-(4-octadecyloxyphenyl)xanthene

: 111447-39-3
2'-O-(3-methoxy-1,5-dicarbomethoxypentane-3-yl)-4-O-(6-methylpyridine-3-yl)uridine

: 111447-40-6
5'-(9-(4-octadecyloxyphenyl)xanthene-9-yl)-2'-O-(3-methoxy-1,5-dicarbomethoxypentane-3-yl)-4-O-(6-methylpyridine-3-yl)uridine

Guidance literature:: With pyridine; In dichloromethane; for 1h;

Reference yield:

: 1121-78-4
5-Hydroxy-2-methylpyridine

: 111447-40-6
5'-(9-(4-octadecyloxyphenyl)xanthene-9-yl)-2'-O-(3-methoxy-1,5-dicarbomethoxypentane-3-yl)-4-O-(6-methylpyridine-3-yl)uridine

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) triethylamine, 2-mesitylenesulfonyl chloride, 4-N,N-dimethylaminopyridine, 2.) 1,4-diazabicyclo<2.2.2>octane, triethylamine / 1.) dichloromethane, 90 min, 2.) dichloromethane, 30 min

2: 0.82 g / tetrabutylammonium fluoride / tetrahydrofuran / 0.03 h

3: 83 percent / pyridine / CH₂Cl₂ / 1 h

With pyridine; 1,4-diaza-bicyclo[2.2.2]octane; dmap; 2-mesitylenesulphonyl chloride; tetrabutyl ammonium fluoride; triethylamine; In tetrahydrofuran; dichloromethane;

Reference yield:

: 3-methoxy-1,5-dicarbomethoxy-2-pentene

: 111447-40-6
5'-(9-(4-octadecyloxyphenyl)xanthene-9-yl)-2'-O-(3-methoxy-1,5-dicarbomethoxypentane-3-yl)-4-O-(6-methylpyridine-3-yl)uridine

Guidance literature:: Multi-step reaction with 4 steps

1: benzenesulfonic acid / dioxane; toluene / 0.08 h

2: 1.) triethylamine, 2-mesitylenesulfonyl chloride, 4-N,N-dimethylaminopyridine, 2.) 1,4-diazabicyclo<2.2.2>octane, triethylamine / 1.) dichloromethane, 90 min, 2.) dichloromethane, 30 min

3: 0.82 g / tetrabutylammonium fluoride / tetrahydrofuran / 0.03 h

4: 83 percent / pyridine / CH₂Cl₂ / 1 h

With pyridine; 1,4-diaza-bicyclo[2.2.2]octane; dmap; 2-mesitylenesulphonyl chloride; tetrabutyl ammonium fluoride; triethylamine; benzenesulfonic acid; In tetrahydrofuran; 1,4-dioxane; dichloromethane; toluene;