Phenol, 2-iodo-6-methoxy-4-methyl-

Base Information

Chemical Name:Phenol, 2-iodo-6-methoxy-4-methyl-
CAS No.:111726-48-8
Molecular Formula:C8H9IO2
Molecular Weight:264.063
Hs Code.:
DSSTox Substance ID:DTXSID50464476
Wikidata:Q82289803

Synonyms:Phenol, 2-iodo-6-methoxy-4-methyl-;111726-48-8;2-IODO-6-METHOXY-4-METHYLPHENOL;SCHEMBL12584694;DTXSID50464476

Suppliers and Price of Phenol, 2-iodo-6-methoxy-4-methyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of Phenol, 2-iodo-6-methoxy-4-methyl-

Chemical Property:

XLogP3:2.6
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:263.96473
Heavy Atom Count:11
Complexity:129

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC(=C(C(=C1)I)O)OC

Technology Process of Phenol, 2-iodo-6-methoxy-4-methyl-

There total 8 articles about Phenol, 2-iodo-6-methoxy-4-methyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 93-51-6
2-Methoxy-4-methylphenol

: 111726-48-8
2-iodo-6-methoxy-4-methylphenol

Guidance literature:: 2-Methoxy-4-methylphenol; With iodine; potassium hydroxide; In methanol; at -78 - 20 ℃; for 0.5h;

With hydrogenchloride; In methanol; water; at 0 ℃;
DOI:10.1002/asia.201100187

Reference yield:

: 4-bromomethyl-2-iodo-6-methoxy-phenol

: 111726-48-8
2-iodo-6-methoxy-4-methylphenol

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether; dichloromethane; at 20 ℃; for 2.5h;
DOI:10.1021/ja001455r

Reference yield:

: 37987-21-6
4-hydroxy-3-iodo-5-methoxybenzyl alcohol

: 111726-48-8
2-iodo-6-methoxy-4-methylphenol

Guidance literature:: Multi-step reaction with 2 steps

1: (CBrCl₂)2; PPh₃ / CH₂Cl₂ / 0 - 20 °C

2: 3.60 g / LiAlH₄ / CH₂Cl₂; diethyl ether / 2.5 h / 20 °C

With lithium aluminium tetrahydride; 1,2-dibromo-1,1,2,2-tetrachloroethane; triphenylphosphine; In diethyl ether; dichloromethane;
DOI:10.1021/ja001455r