(±)-Ochropposinine

Base Information

Chemical Name:(±)-Ochropposinine
CAS No.:37687-31-3
Molecular Formula:C₂₁H₃₀N₂O₃
Molecular Weight:358.481
Hs Code.:
Mol file:37687-31-3.mol

Synonyms:(-)-10,11-Dimethoxycorynan-17-ol;2-((2R,3R,12bS)-3-Ethyl-9,10-dimethoxy-1,2,3,4,6,7,12,12b-octahydro-indolo[2,3-a]quinolizin-2-yl)-ethanol;

Suppliers and Price of (±)-Ochropposinine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (±)-Ochropposinine

Chemical Property:

PSA：57.72000
LogP:3.45070

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of (±)-Ochropposinine

There total 21 articles about (±)-Ochropposinine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 107887-34-3,107887-37-6
(+/-)-10,11-Dimethoxycorynan-17-oic Acid Ethyl Ester

: 37687-31-3,107887-35-4
(+/-)-ochropposinine

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; for 3h; Ambient temperature;
DOI:10.1248/cpb.38.1200 DOI:10.3987/R-1986-05-1215

Reference yield: 81.0%

: 107887-37-6
(-)-10,11-Dimethoxycorynan-17-oic Acid Ethyl Ester

: 37687-31-3
(-)-10,11-Dimethoxycorynan-17-ol

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; for 3h; Ambient temperature;
DOI:10.1248/cpb.38.1200 DOI:10.3987/R-1986-05-1215

Reference yield:

: 81633-43-4
2-Chloro-1-(5,6-dimethoxy-1H-indol-3-yl)ethanone

: 37687-31-3
(-)-10,11-Dimethoxycorynan-17-ol

Guidance literature:: Multi-step reaction with 6 steps

1: 66 percent / KBr / dimethylformamide / 48 h / 60 °C

2: 58 percent / POCl₃ / toluene / 1 h / Heating

3: 60 percent / H₂ / Pt / ethanol / 10 h / 760 Torr / Ambient temperature

4: POCl₃ / toluene / 2 h / Heating

5: H₂ / Pt / ethanol / 4 h / Ambient temperature

6: 81 percent / LiAlH₄ / tetrahydrofuran / 3 h / Ambient temperature

With lithium aluminium tetrahydride; hydrogen; potassium bromide; trichlorophosphate; platinum; In tetrahydrofuran; ethanol; N,N-dimethyl-formamide; toluene;
DOI:10.3987/R-1986-05-1215