1-Hydroxy-3-methylanthracene-9,10-dione

Base Information

Chemical Name:1-Hydroxy-3-methylanthracene-9,10-dione
CAS No.:2549-78-2
Molecular Formula:C15H10 O3
Molecular Weight:238.243
Hs Code.:2914690090
Mol file:2549-78-2.mol

Synonyms:Anthraquinone,1-hydroxy-3-methyl- (6CI,7CI,8CI); 1-Hydroxy-3-methyl-9,10-anthraquinone;1-Hydroxy-3-methylanthraquinone; Pachybasin

Suppliers and Price of 1-Hydroxy-3-methylanthracene-9,10-dione

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
1-Hydroxy-3-methylanthraquinone
1g
$ 1320.00

TRC
1-Hydroxy-3-methylanthraquinone
100mg
$ 165.00

Medical Isotopes, Inc.
1-Hydroxy-3-methylanthraquinone
1 g
$ 2200.00

Cayman Chemical
Pachybasin
1mg
$ 55.00

AK Scientific
9,10-Anthracenedione,1-hydroxy-3-methyl-
1mg
$ 174.00

Total 6 raw suppliers

Chemical Property of 1-Hydroxy-3-methylanthracene-9,10-dione

Chemical Property:

Vapor Pressure:7.94E-09mmHg at 25°C
Melting Point:178 °C(Solv: ethanol (64-17-5))
Boiling Point:453.1°C at 760 mmHg
PKA:7.22±0.20(Predicted)
Flash Point:241.9°C
PSA：54.37000
Density:1.371g/cm³
LogP:2.47600

Purity/Quality:

≥70% ^*data from raw suppliers

1-Hydroxy-3-methylanthraquinone ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Uses 1-Hydroxy-3-methylanthraquinone was found to be involved in the self-regulation of Trichoderma harzianum mycoparasitic coiling.

Technology Process of 1-Hydroxy-3-methylanthracene-9,10-dione

There total 6 articles about 1-Hydroxy-3-methylanthracene-9,10-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.7%

: 85-44-9
phthalic anhydride

: 108-39-4
3-methyl-phenol

: 2549-78-2
pachybasin

Guidance literature:: With aluminum (III) chloride; sodium chloride; at 150 - 170 ℃; for 0.75h;
DOI:10.2174/1570180815666180607085102

Reference yield:

: C₁₅H₁₂O₃

: 2549-78-2
pachybasin

: 84-54-8
2-methylanthracene-9,10-dione

Guidance literature:: With tin (IV) chloride pentahydrate; In dichloromethane; at 20 ℃; for 2h;
DOI:10.1021/acs.joc.7b01987

Reference yield:

: (1,4-dimethoxy-3-(2-methylallyl)naphthalen-2-yl)methanol

: 2549-78-2
pachybasin

: 84-54-8
2-methylanthracene-9,10-dione

Guidance literature:: Multi-step reaction with 3 steps

1: ammonium cerium (IV) nitrate / water; acetonitrile / 1 h / 20 °C

2: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 1 h / 0 - 20 °C

3: tin (IV) chloride pentahydrate / dichloromethane / 2 h / 20 °C

With ammonium cerium (IV) nitrate; tin (IV) chloride pentahydrate; sodium hydrogencarbonate; Dess-Martin periodane; In dichloromethane; water; acetonitrile;
DOI:10.1021/acs.joc.7b01987