Technology Process of Tributyl(1-ethoxy-3-phenylprop-2-YN-1-YL)stannane
There total 1 articles about Tributyl(1-ethoxy-3-phenylprop-2-YN-1-YL)stannane which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
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With
aluminium trichloride; ethylmagnesium bromide;
In
diethyl ether;
Bu3SnCH(OEt)2 reacted with 20% excess of (PhCC)(n)AlX(3-n) obtained from exchange between Grignard reagent (obtained conventionally from PhCCH and EtMgBr) and AlCl3 in Et2O at 20°C;
DOI:10.1039/c39870000029